Simultaneous determination of inorganic anions and cations in explosive residues by ion chromatography
文献类型:期刊论文
作者 | Meng, Hong-Bo ; Wang, Tian-Ran ; Guo, Bao-Yuan ; Hashi, Yuki ; Guo, Can-Xiong ; Lin, Jin-Ming |
刊名 | TALANTA
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出版日期 | 2008-07-15 |
卷号 | 76期号:2页码:241-245 |
关键词 | non-suppressed ion chromatography simultaneously inorganic explosive residues phthalic acid |
英文摘要 | A non-suppressed ion chromatographic method by connecting anion-exchange and cation-exchange columns directly was developed for the separation and determination of five inorganic anions (sulfate, nitrate, chloride, nitrite, and chlorate) and three cations (sodium, ammonium, and potassium) simultaneously in explosive residues. The mobile phase was composed of 3.5 mM phthalic acid with 2% acetonitrile and water at flow rate of 0.2 mL/min. Under the optimal conditions, the eight inorganic ions were completely separated and detected simultaneously within 16 min. The limits of detection (S/N = 3) of the anions and cations were in the range of 50-100 mu g/L and 150-320 mu g/L, respectively, the linear correlation coefficients were 0.9941-0.9996, and the R.S.D. of retention time and peak area were 0.10-0.29% and 5.65-8.12%, respectively. The method was applied successfully to the analysis of the explosive samples with satisfactory results. (C) 2008 Published by Elsevier B.V. |
公开日期 | 2015-08-31 |
源URL | [http://ir.rcees.ac.cn/handle/311016/21992] ![]() |
专题 | 生态环境研究中心_环境化学与生态毒理学国家重点实验室 |
推荐引用方式 GB/T 7714 | Meng, Hong-Bo,Wang, Tian-Ran,Guo, Bao-Yuan,et al. Simultaneous determination of inorganic anions and cations in explosive residues by ion chromatography[J]. TALANTA,2008,76(2):241-245. |
APA | Meng, Hong-Bo,Wang, Tian-Ran,Guo, Bao-Yuan,Hashi, Yuki,Guo, Can-Xiong,&Lin, Jin-Ming.(2008).Simultaneous determination of inorganic anions and cations in explosive residues by ion chromatography.TALANTA,76(2),241-245. |
MLA | Meng, Hong-Bo,et al."Simultaneous determination of inorganic anions and cations in explosive residues by ion chromatography".TALANTA 76.2(2008):241-245. |
入库方式: OAI收割
来源:生态环境研究中心
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