Quantification of Nitroimidazoles Residues in Swine Liver by Liquid Chromatography-Mass Spectrometry with Atmospheric Pressure Chemical Ionization
文献类型:期刊论文
作者 | Wang, Hai; Wang, Zijian; Liu, SuYing; Jiang, Yanbing; Wu, Yinliang; Shan, Jihao |
刊名 | BULLETIN OF ENVIRONMENTAL CONTAMINATION AND TOXICOLOGY
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出版日期 | 2009-04 |
卷号 | 82期号:4页码:411-414 |
关键词 | Nitroimidazoles LC-APCI-MS Swine liver |
中文摘要 | A liquid chromatography-mass spectrometry method was developed for the simultaneous determination of ronidazole (RNZ), metronidazole (MNZ) and dimetridazole (DMZ) residues in swine liver. Following liquid-liquid extraction, the HLB solid-phase extraction was used for further purification. The targets were detected by atmospheric pressure chemical ionization (APCI) following the reverse phase liquid chromatography separation. Consequently, the detection limits for the method were 0.5 mu g/kg for MNZ, 1.0 mu g/kg for RNZ and 0.5 mu g/kg for DMZ, respectively. The accuracies were determined using swine liver samples fortified at levels of 0.5, 1, 2, and 4 mu g/kg and the mean recoveries of the analytes were between 66% and 81%. |
WOS记录号 | WOS:000264514800005 |
源URL | [http://ir.rcees.ac.cn/handle/311016/21726] ![]() |
专题 | 生态环境研究中心_环境水质学国家重点实验室 |
推荐引用方式 GB/T 7714 | Wang, Hai,Wang, Zijian,Liu, SuYing,et al. Quantification of Nitroimidazoles Residues in Swine Liver by Liquid Chromatography-Mass Spectrometry with Atmospheric Pressure Chemical Ionization[J]. BULLETIN OF ENVIRONMENTAL CONTAMINATION AND TOXICOLOGY,2009,82(4):411-414. |
APA | Wang, Hai,Wang, Zijian,Liu, SuYing,Jiang, Yanbing,Wu, Yinliang,&Shan, Jihao.(2009).Quantification of Nitroimidazoles Residues in Swine Liver by Liquid Chromatography-Mass Spectrometry with Atmospheric Pressure Chemical Ionization.BULLETIN OF ENVIRONMENTAL CONTAMINATION AND TOXICOLOGY,82(4),411-414. |
MLA | Wang, Hai,et al."Quantification of Nitroimidazoles Residues in Swine Liver by Liquid Chromatography-Mass Spectrometry with Atmospheric Pressure Chemical Ionization".BULLETIN OF ENVIRONMENTAL CONTAMINATION AND TOXICOLOGY 82.4(2009):411-414. |
入库方式: OAI收割
来源:生态环境研究中心
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