中国科学院机构知识库网格
Chinese Academy of Sciences Institutional Repositories Grid
Continuous-flow microextraction and gas chromatographic-mass spectrometric determination of polycyclic aromatic hydrocarbon compounds in water

文献类型:期刊论文

作者Liu, Yan; Hashi, Yuki; Lin, Jin-Ming
刊名ANALYTICA CHIMICA ACTA
出版日期2007-03-07
卷号585期号:2页码:294-299
关键词continuous-flow microextraction polycyclic aromatic hydrocarbons gas chromatography-mass spectrometry water analysis
英文摘要A new method of the determination polycyclic aromatic hydrocarbons (PAHs) in water samples was developed by continuous-flow microextraction (CFME) coupled with gas chromatography-mass spectrometry (GC-MS). In this experiment, 15 mL sample solution with no salt-added was flowed at the rate of 1.0 mL min(-1) through 3 mu L benzene as extraction solvent. Under the optimal extraction conditions, the developed method was found to yield a linear calibration curve in the concentration range from 0.05 to 15 ng mL(-1). Furthermore, the accuracy and repeatability of the method were good by calculating from water samples spiked at known concentrations of PAHs, and the recovery of optimal method was satisfactory. The results showed that CFME was an efficient preconcentration method for extraction of PAHs from spiked water samples. (c) 2007 Elsevier B.V. All rights reserved.
WOS记录号WOS:000244328100013
源URL[http://ir.rcees.ac.cn/handle/311016/22430]  
专题生态环境研究中心_环境化学与生态毒理学国家重点实验室
推荐引用方式
GB/T 7714
Liu, Yan,Hashi, Yuki,Lin, Jin-Ming. Continuous-flow microextraction and gas chromatographic-mass spectrometric determination of polycyclic aromatic hydrocarbon compounds in water[J]. ANALYTICA CHIMICA ACTA,2007,585(2):294-299.
APA Liu, Yan,Hashi, Yuki,&Lin, Jin-Ming.(2007).Continuous-flow microextraction and gas chromatographic-mass spectrometric determination of polycyclic aromatic hydrocarbon compounds in water.ANALYTICA CHIMICA ACTA,585(2),294-299.
MLA Liu, Yan,et al."Continuous-flow microextraction and gas chromatographic-mass spectrometric determination of polycyclic aromatic hydrocarbon compounds in water".ANALYTICA CHIMICA ACTA 585.2(2007):294-299.

入库方式: OAI收割

来源:生态环境研究中心

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