Determination of sugars and sugar alcohols in tobacco feed liquids by high performance anion-exchange and pulsed amperometric detection
文献类型：期刊论文
| 作者 | Tang Kun-Tian ; Liang Li-Na ; Cai Ya-Qi ; Mon Shifen |
| 刊名 | CHINESE JOURNAL OF ANALYTICAL CHEMISTRY
 |
| 出版日期 | 2007-09 |
| 卷号 | 35期号:9页码:1274-1278 |
| 关键词 | high performance anion exchange chromatography pulsed amperometric detection sugar alcohols sugars tobacco feed liquid |
| 英文摘要 | A chromatographic method was developed for the determination of inositol, galactitol, glycerol, xylitol, propylene glycol, sorbitol, mannitol, glucose, fructose, sucrose, mannose and galactose in tobacco feed liquid samples using high -performance anion-exchange chromatography coupled with pulsed amperometric detection. The separation was carried out on CarboPac MA1 anion-exchange column using NaOH eluent. Moreover, the conditions affecting the separation and detection were optimized. The detection limits ranged from 2. 0 to 7. 6 mu g/L and the linear range of 0. 1 to 50 mg/L was obtained for inositol, galactitol, glycerol, xylitol. The detection limits ranged from 9. 0 to 11. 9 mu g/L and the linear range of I to 50 mg/L was obtained for propylene glycol, sorbitol, mannitol, glucose, mannose and galactose. For fructose and sucrose, the detection limits were 102 mu g/L, 216 mu g/L respectively and linear range was 2 -100 mg/L ( 25. 0 mu L injection, S/N = 3). The RSD of the twelve analytes (1.0 -5. 0 mg/L) was 0.7% -4. 3% (n =7). In addition, the spiked recoveries of the twelve analytes in tobacco feed liquid were 80% -108%. |
| WOS记录号 | WOS:000251296200007 |
| 源URL | [http://ir.rcees.ac.cn/handle/311016/22438]  |
| 专题 | 生态环境研究中心_环境化学与生态毒理学国家重点实验室 |
| 推荐引用方式 GB/T 7714 | Tang Kun-Tian,Liang Li-Na,Cai Ya-Qi,et al. Determination of sugars and sugar alcohols in tobacco feed liquids by high performance anion-exchange and pulsed amperometric detection[J]. CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,2007,35(9):1274-1278. |
| APA | Tang Kun-Tian,Liang Li-Na,Cai Ya-Qi,&Mon Shifen.(2007).Determination of sugars and sugar alcohols in tobacco feed liquids by high performance anion-exchange and pulsed amperometric detection.CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,35(9),1274-1278. |
| MLA | Tang Kun-Tian,et al."Determination of sugars and sugar alcohols in tobacco feed liquids by high performance anion-exchange and pulsed amperometric detection".CHINESE JOURNAL OF ANALYTICAL CHEMISTRY 35.9(2007):1274-1278. |
入库方式： OAI收割
来源：生态环境研究中心
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