Morphology control of self-stacked silicalite-1 crystals using microwave-assisted solvothemial synthesis
文献类型：期刊论文
| 作者 | Chen, Xiaoxin; Yan, Wenfu; Shen, Wanling; Yu, Jihong; Cao, Xuejing; Xu, Ruren |
| 刊名 | MICROPOROUS AND MESOPOROUS MATERIALS
 |
| 出版日期 | 2007-08-23 |
| 卷号 | 104期号:1-3页码:296-304 |
| 关键词 | zeolites MFI microwave radiation solvothermal synthesis morphology |
| 英文摘要 | yMorphology control of silicalite-1 (Si-MFI) crystals was achieved by employing microwave-assisted solvothermal synthesis in the reaction system TEOS-TPAOH-alcohol using dipolar alcohols as a co-solvent. The influences of various experimental parameters, such as dielectric parameters of the alcohols, aging time, and the amount of the alcohols in the reaction mixture on the morphology of the resulting Si-MFI crystals were investigated. Our studies show that self-stacked Si-MFI crystals could be prepared by using alcohols with low dielectric constants as a co-solvent with short aging time and high concentration in the reaction mixture under microwave radiation. The resulting products were further characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), and Si-29 MAS NMR analyses. (C) 2007 Elsevier Inc. All rights reserved. |
| WOS标题词 | Science & Technology ; Physical Sciences ; Technology |
| 类目[WOS] | Chemistry, Applied ; Chemistry, Physical ; Nanoscience & Nanotechnology ; Materials Science, Multidisciplinary |
| 研究领域[WOS] | Chemistry ; Science & Technology - Other Topics ; Materials Science |
| 关键词[WOS] | RAPID SYNTHESIS ; ZEOLITE MEMBRANE ; MOLECULAR-SIEVES ; CRYSTALLIZATION ; NUCLEATION ; CATALYSTS ; ACID |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000249159800036 |
| 公开日期 | 2015-10-13 |
| 源URL | [http://ir.wipm.ac.cn/handle/112942/7901]  |
| 专题 | 武汉物理与数学研究所_2011年以前论文发表（包括2011年） |
| 作者单位 | 1.Jilin Univ, Coll Chem, State Key Lab Inorgan Synth & Preparat Chem, Changchun 130012, Peoples R China 2.Chinese Acad Sci, Wuhan Inst Phys Math, State Key Lab Magnet Resonance & Atom & Mol Phys, Wuhan 430071, Peoples R China |
| 推荐引用方式 GB/T 7714 | Chen, Xiaoxin,Yan, Wenfu,Shen, Wanling,et al. Morphology control of self-stacked silicalite-1 crystals using microwave-assisted solvothemial synthesis[J]. MICROPOROUS AND MESOPOROUS MATERIALS,2007,104(1-3):296-304. |
| APA | Chen, Xiaoxin,Yan, Wenfu,Shen, Wanling,Yu, Jihong,Cao, Xuejing,&Xu, Ruren.(2007).Morphology control of self-stacked silicalite-1 crystals using microwave-assisted solvothemial synthesis.MICROPOROUS AND MESOPOROUS MATERIALS,104(1-3),296-304. |
| MLA | Chen, Xiaoxin,et al."Morphology control of self-stacked silicalite-1 crystals using microwave-assisted solvothemial synthesis".MICROPOROUS AND MESOPOROUS MATERIALS 104.1-3(2007):296-304. |
入库方式： OAI收割
来源：武汉物理与数学研究所
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