A novel amide stationary phase for hydrophilic interaction liquid chromatography and ion chromatography
文献类型:期刊论文
作者 | Shen, Guobin1; Zhang, FeiFang1; Yang, Bingcheng1; Chu, Changhu1; Liang, Xinmiao1,2 |
刊名 | talanta
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出版日期 | 2013-10-15 |
卷号 | 115页码:129-132 |
关键词 | Hydrophilic interaction liquid chromatography Amide stationary phase Ion chromatography Click chemistry |
英文摘要 | a novel amide stationary phase (asp) for hydrophilic interaction liquid chromatography (hilic) has been prepared via the click chemistry method. it was based on the strategy that the amino group of asparagine was easily transferred to the corresponding azido group and then clicked onto terminal alkyne-silica gel in the presence of cu(i)-based catalyst. for the tested polar compounds including nucleosides and nucleic acid bases, asp-based column has demonstrated good performance in terms of separation efficiency and column stability, and the retention mechanism was found to match well the typical hilic retention. in addition, the asp described here showed much better selectivity in separation of inorganic anions under ion chromatography mode relative to other kinds of commercial asp. (c) 2013 elsevier b.v. all rights reserved. |
WOS标题词 | science & technology ; physical sciences |
类目[WOS] | chemistry, analytical |
研究领域[WOS] | chemistry |
关键词[WOS] | inorganic anions ; separation ; exchange ; column |
收录类别 | SCI |
语种 | 英语 |
WOS记录号 | WOS:000328095600016 |
公开日期 | 2015-11-10 |
源URL | [http://159.226.238.44/handle/321008/137478] ![]() |
专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
作者单位 | 1.E China Univ Sci & Technol, Sch Pharm, Shanghai 200237, Peoples R China 2.Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116023, Peoples R China |
推荐引用方式 GB/T 7714 | Shen, Guobin,Zhang, FeiFang,Yang, Bingcheng,et al. A novel amide stationary phase for hydrophilic interaction liquid chromatography and ion chromatography[J]. talanta,2013,115:129-132. |
APA | Shen, Guobin,Zhang, FeiFang,Yang, Bingcheng,Chu, Changhu,&Liang, Xinmiao.(2013).A novel amide stationary phase for hydrophilic interaction liquid chromatography and ion chromatography.talanta,115,129-132. |
MLA | Shen, Guobin,et al."A novel amide stationary phase for hydrophilic interaction liquid chromatography and ion chromatography".talanta 115(2013):129-132. |
入库方式: OAI收割
来源:大连化学物理研究所
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