Novel fluorescence derivatization reagent for the determination of alcohol by high performance liquid chromatography and fluorescent detection
文献类型:期刊论文
作者 | Chen, GF; You, JM; Zhang, YK |
刊名 | chinese journal of analytical chemistry
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出版日期 | 2003 |
卷号 | 31期号:1页码:62-65 |
关键词 | 2-(9-carbazole)-ethyl chloroformate high performance liquid chromatography pre-column derivatization alcohols |
英文摘要 | a novel fluorescence and ultraviolet labelling reagent, 2-(9-carbazole)-ethyl chloroformate, has been utilized as pre-column derivatization reagent for 15 aliphatic alcohols. the optimal derivatization conditions were investigated,. the results indicate that the derivatizing temperature is at 80degreesc and reaction time is 15 min and pyridine is used as catalyst. high performance liquid chromatography coupled with fluorescence detector was studied as a means of separation and determination of alcohols. the derivative baseline resolution has been acuired by optimizing separation condition. the limit of detection is 13.3similar to93.5 nmol/l. |
WOS标题词 | science & technology ; physical sciences |
类目[WOS] | chemistry, analytical |
研究领域[WOS] | chemistry |
关键词[WOS] | methanol ; ethanol |
收录类别 | SCI |
语种 | 英语 |
WOS记录号 | WOS:000180964300016 |
公开日期 | 2015-11-10 |
源URL | [http://159.226.238.44/handle/321008/138392] ![]() |
专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
作者单位 | Acad Sinica, Dalian Inst Chem Phys, Natl Chromatog Res & Anal Ctr, Dalian 116011, Peoples R China |
推荐引用方式 GB/T 7714 | Chen, GF,You, JM,Zhang, YK. Novel fluorescence derivatization reagent for the determination of alcohol by high performance liquid chromatography and fluorescent detection[J]. chinese journal of analytical chemistry,2003,31(1):62-65. |
APA | Chen, GF,You, JM,&Zhang, YK.(2003).Novel fluorescence derivatization reagent for the determination of alcohol by high performance liquid chromatography and fluorescent detection.chinese journal of analytical chemistry,31(1),62-65. |
MLA | Chen, GF,et al."Novel fluorescence derivatization reagent for the determination of alcohol by high performance liquid chromatography and fluorescent detection".chinese journal of analytical chemistry 31.1(2003):62-65. |
入库方式: OAI收割
来源:大连化学物理研究所
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