Structural identification of human blood phospholipids using liquid chromatography/quadrupole-linear ion trap mass spectrometry
文献类型：期刊论文
| 作者 | Wang, C; Xie, SG; Yang, J; Yang, Q; Xu, GW |
| 刊名 | analytica chimica acta
 |
| 出版日期 | 2004-11-01 |
| 卷号 | 525期号:1页码:1-10 |
| 关键词 | phospholipids linear ion trap ionspray liquid chromatography/mass spectrometry |
| 英文摘要 | a normal-phase liquid chromatography/quadrupole-linear ion trap mass spectrometry method was developed for the separation and mass spectral characterization of the main phospholipid species in human blood. the instrument combines the capabilities of a triple quadrupole mass spectrometer and ion trap technology on a single platform. the optimal separation was achieved by using hexane/1-propanol as mobile phase and 0.6% formic acid, 0.06% ammonia as modifiers. the hplc/ms technique was able to provide information about the molecular mass of individual homologues by positive and negative turbo ionspray. more complete characterization of fatty acid chains and of the polar head group was obtained by using a quadrupole collisionally activated dissociation (cad) spectrum with ion trap sensitivity. the mass spectra and molecular species of phosphatidylserine (ps), phosphatidylethanolamine (pe), phosphatidylcholine (pc), lysophosphatidylcholine (lysopc) and sphingomyelin (sm) are presented. (c) 2004 elsevier b.v. all rights reserved. |
| WOS标题词 | science & technology ; physical sciences |
| 类目[WOS] | chemistry, analytical |
| 研究领域[WOS] | chemistry |
| 关键词[WOS] | collision-induced dissociation ; light-scattering detection ; electrospray-ionization ; gas-chromatography ; class separation ; cooked beef ; glycerophospholipids ; phosphatidylcholine ; lecithins ; detector |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000224593600001 |
| 公开日期 | 2015-11-10 |
| 源URL | [http://159.226.238.44/handle/321008/138407]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | 1.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatog R&A Ctr, Dalian 116011, Peoples R China 2.Dalian Ctr Hosp, Dalian 116033, Peoples R China |
| 推荐引用方式 GB/T 7714 | Wang, C,Xie, SG,Yang, J,et al. Structural identification of human blood phospholipids using liquid chromatography/quadrupole-linear ion trap mass spectrometry[J]. analytica chimica acta,2004,525(1):1-10. |
| APA | Wang, C,Xie, SG,Yang, J,Yang, Q,&Xu, GW.(2004).Structural identification of human blood phospholipids using liquid chromatography/quadrupole-linear ion trap mass spectrometry.analytica chimica acta,525(1),1-10. |
| MLA | Wang, C,et al."Structural identification of human blood phospholipids using liquid chromatography/quadrupole-linear ion trap mass spectrometry".analytica chimica acta 525.1(2004):1-10. |
入库方式： OAI收割
来源：大连化学物理研究所
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