Determination of the active ingredients in Rhizoma Chuanxiong by high performance liquid chromatography-mass spectrometry
文献类型:期刊论文
作者 | Kong, LA; Yu, ZY; Zou, HF; Sun, NC; Wu, LH; Ni, JY |
刊名 | chinese journal of analytical chemistry
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出版日期 | 2004-11-01 |
卷号 | 32期号:11页码:1501-1504 |
关键词 | high performance liquid chromatography-mass spectrometry Rhizoma Chuanxiong quality control ferulic acid ligustilide |
英文摘要 | the main active ingredients, ferulic acid. and ligustilide in chinese traditional medicine, rhizoma chuanxiong, were separated and identified by high performance liquid chromatography-mass sepctrum (hplc-ms). the standard ligustilide was prepared with preparative scale hplc and identified by hplc-diode array detection, mass spectrometry, infrared spectroscopy. four kinds of extractiting solvent and extraction time affecting on the extraction efficiency of ferulic acid and ligustilide in rhizoma chuanxiong were examined, and a quality control method was also developed based on the quantitative determination of ferulic acid and liguistilide in extracted solutions of rhizoma chuanxiong by water and ethanol. the amount of ferulic acid and ligustilide in rhizoma chuanxiong determined are as much as 0.15% ( w/w) and 0.82% (w/w). |
WOS标题词 | science & technology ; physical sciences |
类目[WOS] | chemistry, analytical |
研究领域[WOS] | chemistry |
收录类别 | SCI |
语种 | 英语 |
WOS记录号 | WOS:000225615700021 |
公开日期 | 2015-11-10 |
源URL | [http://159.226.238.44/handle/321008/138450] ![]() |
专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
作者单位 | Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatograph Res & Anal Ctr, Dalian 116011, Peoples R China |
推荐引用方式 GB/T 7714 | Kong, LA,Yu, ZY,Zou, HF,et al. Determination of the active ingredients in Rhizoma Chuanxiong by high performance liquid chromatography-mass spectrometry[J]. chinese journal of analytical chemistry,2004,32(11):1501-1504. |
APA | Kong, LA,Yu, ZY,Zou, HF,Sun, NC,Wu, LH,&Ni, JY.(2004).Determination of the active ingredients in Rhizoma Chuanxiong by high performance liquid chromatography-mass spectrometry.chinese journal of analytical chemistry,32(11),1501-1504. |
MLA | Kong, LA,et al."Determination of the active ingredients in Rhizoma Chuanxiong by high performance liquid chromatography-mass spectrometry".chinese journal of analytical chemistry 32.11(2004):1501-1504. |
入库方式: OAI收割
来源:大连化学物理研究所
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