Preparation and evaluation of high efficient rod-shape poly(methacrylic acid-styrene-divinylbenzene) high performance liquid chromatographic column
文献类型:期刊论文
作者 | Wang, JF; Meng, ZH; Zhou, LM; Wang, QH; Zhu, DQ |
刊名 | chinese journal of analytical chemistry
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出版日期 | 1999-07-01 |
卷号 | 27期号:7页码:745-748 |
关键词 | high performance liquid chromatography column in situ polymerization (methacrylic acid-styrene-divinylbenzene) copolymer polycyclic aromatic hydrocarbons |
英文摘要 | a novel high efficiency rod-shape poly(methacrylic acid-co-styrene-co-divinylbenzene) high performance liquid chromatographic column was prepared by a free-radical polymerization directly within the column. scanning electron micrograph revealed the macropores of the copolymer column media. it had excellent permeability and the column pressure was only 2.5 mpa at a flow-rate of 2.0 ml/min with acetonitrile-water (90/10, v/v) as mobile phase. it also showed the rather high efficiency with the theoretical plates being 40,000 plates per meter. aromatic acids and polycyclic aromatic hydrocarbons were separated within 4 and 10 minutes, respectively. |
WOS标题词 | science & technology ; physical sciences |
类目[WOS] | chemistry, analytical |
研究领域[WOS] | chemistry |
关键词[WOS] | reversed-phase chromatography ; separation medium ; macroporous poly(styrene-co-divinylbenzene) ; monolithic rod ; polymers |
收录类别 | SCI |
语种 | 英语 |
WOS记录号 | WOS:000081672300001 |
公开日期 | 2015-11-10 |
源URL | [http://159.226.238.44/handle/321008/138568] ![]() |
专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
作者单位 | Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116012, Peoples R China |
推荐引用方式 GB/T 7714 | Wang, JF,Meng, ZH,Zhou, LM,et al. Preparation and evaluation of high efficient rod-shape poly(methacrylic acid-styrene-divinylbenzene) high performance liquid chromatographic column[J]. chinese journal of analytical chemistry,1999,27(7):745-748. |
APA | Wang, JF,Meng, ZH,Zhou, LM,Wang, QH,&Zhu, DQ.(1999).Preparation and evaluation of high efficient rod-shape poly(methacrylic acid-styrene-divinylbenzene) high performance liquid chromatographic column.chinese journal of analytical chemistry,27(7),745-748. |
MLA | Wang, JF,et al."Preparation and evaluation of high efficient rod-shape poly(methacrylic acid-styrene-divinylbenzene) high performance liquid chromatographic column".chinese journal of analytical chemistry 27.7(1999):745-748. |
入库方式: OAI收割
来源:大连化学物理研究所
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