Preparation and evaluation of stainless-steel wide-bore packed capillary high performance liquid chromatographic columns
文献类型：期刊论文
| 作者 | Tang, YH; Zhu, DQ; Guan, YF |
| 刊名 | chinese journal of analytical chemistry
 |
| 出版日期 | 2001-10-01 |
| 卷号 | 29期号:10页码:1228-1232 |
| 关键词 | packed capillary liquid chromatographic column column preparation column end structure packing reservoir |
| 英文摘要 | the zero-dead volume union ends and conical slurry reservoir for microbore columns were designed. a detailed procedure for the preparation of highly efficient and stable stainless-steel microbore columns with reversed-phase ods is described. the influence of packing direction, packing solvent, slurry solvent, slurry concentration and packing pressure has been studied systematically. columns with efficiency of 75,000/m (number of theoretical plate) were prepared reproducibly at 40mpa packing pressure and optimized conditions. the peak asymmetric factor was 1.03 similar to 1.10 for all the compounds tested. |
| WOS标题词 | science & technology ; physical sciences |
| 类目[WOS] | chemistry, analytical |
| 研究领域[WOS] | chemistry |
| 关键词[WOS] | microbore columns ; packing |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000171887300030 |
| 公开日期 | 2015-11-10 |
| 源URL | [http://159.226.238.44/handle/321008/138889]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116012, Peoples R China |
| 推荐引用方式 GB/T 7714 | Tang, YH,Zhu, DQ,Guan, YF. Preparation and evaluation of stainless-steel wide-bore packed capillary high performance liquid chromatographic columns[J]. chinese journal of analytical chemistry,2001,29(10):1228-1232. |
| APA | Tang, YH,Zhu, DQ,&Guan, YF.(2001).Preparation and evaluation of stainless-steel wide-bore packed capillary high performance liquid chromatographic columns.chinese journal of analytical chemistry,29(10),1228-1232. |
| MLA | Tang, YH,et al."Preparation and evaluation of stainless-steel wide-bore packed capillary high performance liquid chromatographic columns".chinese journal of analytical chemistry 29.10(2001):1228-1232. |
入库方式： OAI收割
来源：大连化学物理研究所
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