Analysis of terpene compounds in Cimicifuga foetida L. by reversed-phase high-performance liquid chromatography with evaporative light scattering detection
文献类型：期刊论文
| 作者 | Kong, L; Li, X; Zou, HF; Wang, HL; Mao, XQ; Zhang, Q; Ni, JY |
| 刊名 | journal of chromatography a
 |
| 出版日期 | 2001-11-30 |
| 卷号 | 936期号:1-2页码:111-118 |
| 关键词 | Cimicifuga foetida L. pharmaceutical analysis terpenes |
| 英文摘要 | an rp-hplc method with evaporative light scattering detection (elsd) was developed for the analysis of terpene compounds in traditional chinese medicine. actein, 27-deoxyactein and cimicifugoside in a typical chinese medicine of cimicifuga foetida l. were quantitatively analyzed. comparing elsd with uv detection under the same eluent conditions, the former showed better sensitivity and a more stable baseline. the elsd responses versus sample size of three terpenes and those in double logarithmic were investigated. the good calibration curves in double logarithmic coordinator for actein, 27-deoxyactein and cimicifugoside were obtained. three solutions for the extraction of the terpene compounds were also compared, the results indicated that methanol-water (80:20) is the best among them. the method was applied to quantify actein, 27-deoxyactein and cimicifugoside in cimicifuga foetida l. from hunan, china. it was shown that elsd is an effective detection method for the analysis of the non-volatile terpenes in traditional chinese medicine. (c) 2001 elsevier science b.v. all rights reserved. |
| WOS标题词 | science & technology ; life sciences & biomedicine ; physical sciences |
| 类目[WOS] | biochemical research methods ; chemistry, analytical |
| 研究领域[WOS] | biochemistry & molecular biology ; chemistry |
| 关键词[WOS] | mass detector ; column |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000172320100009 |
| 公开日期 | 2015-11-10 |
| 源URL | [http://159.226.238.44/handle/321008/138908]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatog R&A Ctr, Dalian 116011, Peoples R China |
| 推荐引用方式 GB/T 7714 | Kong, L,Li, X,Zou, HF,et al. Analysis of terpene compounds in Cimicifuga foetida L. by reversed-phase high-performance liquid chromatography with evaporative light scattering detection[J]. journal of chromatography a,2001,936(1-2):111-118. |
| APA | Kong, L.,Li, X.,Zou, HF.,Wang, HL.,Mao, XQ.,...&Ni, JY.(2001).Analysis of terpene compounds in Cimicifuga foetida L. by reversed-phase high-performance liquid chromatography with evaporative light scattering detection.journal of chromatography a,936(1-2),111-118. |
| MLA | Kong, L,et al."Analysis of terpene compounds in Cimicifuga foetida L. by reversed-phase high-performance liquid chromatography with evaporative light scattering detection".journal of chromatography a 936.1-2(2001):111-118. |
入库方式： OAI收割
来源：大连化学物理研究所
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