Fast optimization method of binary multi-segment gradient elution conditions for the separation of complex samples in reversed phase-high performance liquid chromatography
文献类型：期刊论文
| 作者 | Shan, YC; Zhao, RH; Zhang, WB; Liang, Z; Zhang, YK |
| 刊名 | chinese journal of analytical chemistry
 |
| 出版日期 | 2002-12-01 |
| 卷号 | 30期号:12页码:1444-1447 |
| 关键词 | high performance liquid chromatography retention equation linear gradient stepwise gradient overlapping separation range mapping |
| 英文摘要 | a novel method for the fast optimization of binary multi-step gradient elution in reversed phase-high performance liquid chromatography was proposed. the retention equation of solutes can be obtained by running several linear gradient elutions and then the multi-step gradient elution was optimized using: them overlapping separation range mapping (osrm only several hours were needed to complete the optimization process. this method was validated by the separation of chinese medicine chuanxiong extract,. in which good prediction precision and separation performance were obtained. |
| WOS标题词 | science & technology ; physical sciences |
| 类目[WOS] | chemistry, analytical |
| 研究领域[WOS] | chemistry |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000180173400009 |
| 公开日期 | 2015-11-10 |
| 源URL | [http://159.226.238.44/handle/321008/139075]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116011, Peoples R China |
| 推荐引用方式 GB/T 7714 | Shan, YC,Zhao, RH,Zhang, WB,et al. Fast optimization method of binary multi-segment gradient elution conditions for the separation of complex samples in reversed phase-high performance liquid chromatography[J]. chinese journal of analytical chemistry,2002,30(12):1444-1447. |
| APA | Shan, YC,Zhao, RH,Zhang, WB,Liang, Z,&Zhang, YK.(2002).Fast optimization method of binary multi-segment gradient elution conditions for the separation of complex samples in reversed phase-high performance liquid chromatography.chinese journal of analytical chemistry,30(12),1444-1447. |
| MLA | Shan, YC,et al."Fast optimization method of binary multi-segment gradient elution conditions for the separation of complex samples in reversed phase-high performance liquid chromatography".chinese journal of analytical chemistry 30.12(2002):1444-1447. |
入库方式： OAI收割
来源：大连化学物理研究所
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