Synthesis, characterization and evaluation of a novel double-amine packing for reversed-phage high performance liquid chromatography
文献类型：期刊论文
| 作者 | Huang, XJ; Wang, JD; Liu, XL; Cong, RZ |
| 刊名 | chinese journal of analytical chemistry
 |
| 出版日期 | 2002-09-01 |
| 卷号 | 30期号:9页码:1048-1052 |
| 关键词 | high performance liquid chromatography double-amine stationary phase reversed phase packing |
| 英文摘要 | a novel double-amine packing (dabp) for reversed-phase high performance liquid chromatography (rp-hplc) was synthesized by the reaction of hexyldiamine with beta-(3,4-epoxycyclohexyl) ethyltrimethoxy silane, the intermediate product was coupled onto porous silica to get the intermediate product ii, then the product ii was reacted with octanoyl chloride under catalytst. characterization of the prepared packing was carried out with elemental analysis, solid-state c-13 nuclear magnetic resonance and fourier transform infrared (ff-ir). the chromatographic evaluation was carried out by using organic components including acidic, basic and neutral analytes as probe molecules. the results show that the separate mechanism of basic analytes on the dabp include shydrophobicity and ion repulse. |
| WOS标题词 | science & technology ; physical sciences |
| 类目[WOS] | chemistry, analytical |
| 研究领域[WOS] | chemistry |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000178379800006 |
| 公开日期 | 2015-11-10 |
| 源URL | [http://159.226.238.44/handle/321008/139207]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116012, Peoples R China |
| 推荐引用方式 GB/T 7714 | Huang, XJ,Wang, JD,Liu, XL,et al. Synthesis, characterization and evaluation of a novel double-amine packing for reversed-phage high performance liquid chromatography[J]. chinese journal of analytical chemistry,2002,30(9):1048-1052. |
| APA | Huang, XJ,Wang, JD,Liu, XL,&Cong, RZ.(2002).Synthesis, characterization and evaluation of a novel double-amine packing for reversed-phage high performance liquid chromatography.chinese journal of analytical chemistry,30(9),1048-1052. |
| MLA | Huang, XJ,et al."Synthesis, characterization and evaluation of a novel double-amine packing for reversed-phage high performance liquid chromatography".chinese journal of analytical chemistry 30.9(2002):1048-1052. |
入库方式： OAI收割
来源：大连化学物理研究所
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