Preparation and evaluation of alkyl-amine reversed phase high performance liquid chromatographic packing
文献类型：期刊论文
| 作者 | Huang, XJ; Wang, JD; Liu, XL; Cong, RZ |
| 刊名 | chinese journal of analytical chemistry
 |
| 出版日期 | 2002-08-01 |
| 卷号 | 30期号:8页码:962-966 |
| 关键词 | silane coupling agent alkyl-amine reversed phase packing reversed phase liquid chromatography basic compounds separation |
| 英文摘要 | a new silane coupling agent-beta-(3,4-epoxycyclohexyl) ethyltrimethoxy silane was firstly used to react with octylamine, then the intermediate product was coupled onto porous silica to obtain a novel bonded phase for reversed-phase high performance liquid chromatography. characterization of prepared packing was carried out with elemental analysis, solid-state c-13 nuclear magnetic resonance, fourier transform infrared (ft-ir). chromatographic evaluations were carried out by using a mixture of organic compounds including acidic, basic and neutral analytes and methanol-water as binary mobile phase. the results show that the stationary phase has excellent chromatographic properties and can resist stably on hydrolyzing between ph = 2 similar to 8. it can be efficiently used for the separation of basic compounds. |
| WOS标题词 | science & technology ; physical sciences |
| 类目[WOS] | chemistry, analytical |
| 研究领域[WOS] | chemistry |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000177806100017 |
| 公开日期 | 2015-11-10 |
| 源URL | [http://159.226.238.44/handle/321008/139232]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116012, Peoples R China |
| 推荐引用方式 GB/T 7714 | Huang, XJ,Wang, JD,Liu, XL,et al. Preparation and evaluation of alkyl-amine reversed phase high performance liquid chromatographic packing[J]. chinese journal of analytical chemistry,2002,30(8):962-966. |
| APA | Huang, XJ,Wang, JD,Liu, XL,&Cong, RZ.(2002).Preparation and evaluation of alkyl-amine reversed phase high performance liquid chromatographic packing.chinese journal of analytical chemistry,30(8),962-966. |
| MLA | Huang, XJ,et al."Preparation and evaluation of alkyl-amine reversed phase high performance liquid chromatographic packing".chinese journal of analytical chemistry 30.8(2002):962-966. |
入库方式： OAI收割
来源：大连化学物理研究所
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