Enantiomer separation of dimethyl dicarboxy alpha-biphenyl (DDB) and its analogues on a covalently bonded cellulose tris-(3,5-dimethylphenyl-carbamate) CSP
文献类型:期刊论文
作者 | Qin, F; Chen, XM; Liu, YQ; Kong, L; Zou, HF |
刊名 | journal of separation science
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出版日期 | 2004-10-01 |
卷号 | 27期号:14页码:1195-1201 |
关键词 | enantiomeric separation mobile phase modifiers bonded type of CSP dimethyl dicarboxy biphenyl liquid chromatography |
英文摘要 | dimethyl dicarboxy a-biphenyl (ddb) and its analogues represent atropisomers which have been resolved on the covalently bonded cellulose tris-(3,5-dimethylphenylcarbamate) (cdmpc) csp. different kinds of alcohols, tetrahydrofuran (thf), and chloroform were employed as mobile phase modifiers (mpms), and their influence on the retention and separation of the enantiomers was investigated. ternary mobile phases (hexane/2-propanol/thf, hexane/2-propanol/chloroform) were employed to investigate the separation of the five enantiomers. the advantages of the broader choice of solvents offered by the covalently bonded cdmpc csp were discussed. the effect of structural variation of the enantiomers on their retention and separation was investigated. |
WOS标题词 | science & technology ; physical sciences |
类目[WOS] | chemistry, analytical |
研究领域[WOS] | chemistry |
关键词[WOS] | chiral stationary phases ; performance liquid-chromatography ; silica-gel ; resolution ; derivatives ; tris(3,5-dimethylphenylcarbamate) ; ellagitannin |
收录类别 | SCI |
语种 | 英语 |
WOS记录号 | WOS:000224783400007 |
公开日期 | 2015-11-10 |
源URL | [http://159.226.238.44/handle/321008/139592] ![]() |
专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
作者单位 | Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatog Res & Anal Ctr, Dalian 116011, Peoples R China |
推荐引用方式 GB/T 7714 | Qin, F,Chen, XM,Liu, YQ,et al. Enantiomer separation of dimethyl dicarboxy alpha-biphenyl (DDB) and its analogues on a covalently bonded cellulose tris-(3,5-dimethylphenyl-carbamate) CSP[J]. journal of separation science,2004,27(14):1195-1201. |
APA | Qin, F,Chen, XM,Liu, YQ,Kong, L,&Zou, HF.(2004).Enantiomer separation of dimethyl dicarboxy alpha-biphenyl (DDB) and its analogues on a covalently bonded cellulose tris-(3,5-dimethylphenyl-carbamate) CSP.journal of separation science,27(14),1195-1201. |
MLA | Qin, F,et al."Enantiomer separation of dimethyl dicarboxy alpha-biphenyl (DDB) and its analogues on a covalently bonded cellulose tris-(3,5-dimethylphenyl-carbamate) CSP".journal of separation science 27.14(2004):1195-1201. |
入库方式: OAI收割
来源:大连化学物理研究所
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