Preparation of silica-bonded bovine serum albumin chiral monolithic column for enantiomeric separation by capillary electrochromatography
文献类型：期刊论文
| 作者 | Yan, LJ; Zhang, QH; Zhang, WB; Feng, YQ; Zhang, LH; Li, T; Zhang, YK |
| 刊名 | chemical journal of chinese universities-chinese
 |
| 出版日期 | 2005-05-10 |
| 卷号 | 26期号:5页码:835-837 |
| 关键词 | capillary electrochromatography(CEC) monolithic column sol-gel chiral stationary phases (CSps) bovine serum albumin (BSA) |
| 英文摘要 | a silica-bonded bovine serum albumin (bsa) chiral monolithic stationary phase for capillary electrochromatography(cec) was introduced. an inorganic-organic hybrid monolithic column was firstly prepared by sol-gel chemistry with homogeneously distributed aminopropyl groups throughout the silica matrix. then the chiral stationary phase was synthesized by the in situ covalent immobilization of bsa on the monolithic column activated with glutaraldehyde. the effects of ph value and concentration of phosphate buffer on the separation of d,l-tryptophan were investigated. the separation factor of d,l-tryptophan reached 3.37 on cec mode. |
| WOS标题词 | science & technology ; physical sciences |
| 类目[WOS] | chemistry, multidisciplinary |
| 研究领域[WOS] | chemistry |
| 关键词[WOS] | sol-gel process |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000229296100012 |
| 公开日期 | 2015-11-10 |
| 源URL | [http://159.226.238.44/handle/321008/139822]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | 1.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatog Res & Anal Ctr, Dalian 116023, Peoples R China 2.Wuhan Univ, Coll Chem & Mol Sci, Wuhan 430072, Peoples R China 3.Dalian Elite Analyt Instruments Co Ltd, Dalian 116011, Peoples R China |
| 推荐引用方式 GB/T 7714 | Yan, LJ,Zhang, QH,Zhang, WB,et al. Preparation of silica-bonded bovine serum albumin chiral monolithic column for enantiomeric separation by capillary electrochromatography[J]. chemical journal of chinese universities-chinese,2005,26(5):835-837. |
| APA | Yan, LJ.,Zhang, QH.,Zhang, WB.,Feng, YQ.,Zhang, LH.,...&Zhang, YK.(2005).Preparation of silica-bonded bovine serum albumin chiral monolithic column for enantiomeric separation by capillary electrochromatography.chemical journal of chinese universities-chinese,26(5),835-837. |
| MLA | Yan, LJ,et al."Preparation of silica-bonded bovine serum albumin chiral monolithic column for enantiomeric separation by capillary electrochromatography".chemical journal of chinese universities-chinese 26.5(2005):835-837. |
入库方式： OAI收割
来源：大连化学物理研究所
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