Preparation of solid phase on stir bar for sorptive extraction by sol-gel method
文献类型：期刊论文
| 作者 | Liu, WM; Wang, HW; Guan, YF |
| 刊名 | chinese journal of analytical chemistry
 |
| 出版日期 | 2005 |
| 卷号 | 33期号:1页码:45-49 |
| 关键词 | sol-gel solid phase microextraction stir bar sorptive extraction n-alkanes polyaromatic hydrocarbons |
| 英文摘要 | a sol-gel coating-method for the preparation of coating film on bars used in sorptive microextraction is described. the poly( dimethysiloane) (pdms) is partially crosslinked with the sol-gel network, and the most. part is entangled within the network. three step aging temperatures are applied for the sol-gel coating layer to avoid caking of the film. the thickness of extraction phase is 30 mum, and can be increased by way of multi-coating. the extraction phase prepared by using the improved coating technology shows good thermal stability up to 300degreesc. the analyses of spiked aqueous samples containing n-alkanes or polyaromatic hydrocarbons, were carried out by using the sorptive bars and gas chromatography, which, demonstrated the applicability of the method. |
| WOS标题词 | science & technology ; physical sciences |
| 类目[WOS] | chemistry, analytical |
| 研究领域[WOS] | chemistry |
| 关键词[WOS] | microcolumn-liquid-chromatography ; capillary gas-chromatography ; mass-spectrometry ; aqueous samples ; water samples ; microextraction ; gc ; hydrocarbons |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000226805000011 |
| 公开日期 | 2015-11-10 |
| 源URL | [http://159.226.238.44/handle/321008/139836]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116012, Peoples R China |
| 推荐引用方式 GB/T 7714 | Liu, WM,Wang, HW,Guan, YF. Preparation of solid phase on stir bar for sorptive extraction by sol-gel method[J]. chinese journal of analytical chemistry,2005,33(1):45-49. |
| APA | Liu, WM,Wang, HW,&Guan, YF.(2005).Preparation of solid phase on stir bar for sorptive extraction by sol-gel method.chinese journal of analytical chemistry,33(1),45-49. |
| MLA | Liu, WM,et al."Preparation of solid phase on stir bar for sorptive extraction by sol-gel method".chinese journal of analytical chemistry 33.1(2005):45-49. |
入库方式： OAI收割
来源：大连化学物理研究所
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