Analysis of flavonoids in leaves of Adinandra nitida by capillary electrochromatography on monolithic columns with stepwise gradient elution
文献类型：期刊论文
| 作者 | Zhang, LY; Zhang, J; Wang, H; Zhang, LH; Zhang, WB; Zhang, YK |
| 刊名 | journal of separation science
 |
| 出版日期 | 2005-05-01 |
| 卷号 | 28期号:8页码:774-779 |
| 关键词 | Adinandra nitida flavonoid quality control monolithic columns capillary electrochromatography |
| 英文摘要 | extracts of adinandra nifida leaves, known as shiyacha in china, were analyzed by monolithic columns of capillary electrochromatography (cec). to obtain good resolution within a short time, stepwise gradient elution of cec was employed, and the effects of experimental parameters, such as the buffer, the gradient conditions, and the mode of injection were studied systematically. under optimized conditions, analysis could be accomplished in 25 min on a monolithic rod of macroporous poly(butyl methacrylate-co-ethylene dimethacrylate). with two identified flavonoids, epicatechin and apigenin, as markers, a quality control method for shiyacha and its relevant products was established. the calibration curves exhibited good linear behavior over the concentration range of two orders of magnitude. on combination with an on-line concentration technique, the detection limit of flavonoids could be decreased to 25 ng for apigenin. |
| WOS标题词 | science & technology ; physical sciences |
| 类目[WOS] | chemistry, analytical |
| 研究领域[WOS] | chemistry |
| 关键词[WOS] | ionization-mass-spectrometry ; liquid-chromatography ; separation media ; stationary ; proteins ; phases ; fruits ; rods ; uv |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000229404700010 |
| 公开日期 | 2015-11-10 |
| 源URL | [http://159.226.238.44/handle/321008/139911]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromotog Res & Anal Ctr, Dalian 116023, Peoples R China |
| 推荐引用方式 GB/T 7714 | Zhang, LY,Zhang, J,Wang, H,et al. Analysis of flavonoids in leaves of Adinandra nitida by capillary electrochromatography on monolithic columns with stepwise gradient elution[J]. journal of separation science,2005,28(8):774-779. |
| APA | Zhang, LY,Zhang, J,Wang, H,Zhang, LH,Zhang, WB,&Zhang, YK.(2005).Analysis of flavonoids in leaves of Adinandra nitida by capillary electrochromatography on monolithic columns with stepwise gradient elution.journal of separation science,28(8),774-779. |
| MLA | Zhang, LY,et al."Analysis of flavonoids in leaves of Adinandra nitida by capillary electrochromatography on monolithic columns with stepwise gradient elution".journal of separation science 28.8(2005):774-779. |
入库方式： OAI收割
来源：大连化学物理研究所
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