Analysis of volatile and semi-volatile alkaline compounds in tobacco leaf by using comprehensive two-dimensional gas chromatography/time-of-flight mass spectrometry
文献类型:期刊论文
作者 | Li Hai-Feng; Zhong Ke-Jun; Lu Xin; Bai Chang-Min; Huang Jian-Guo; Lu Hong-Liang; Ma Chen-Fei; Zhu Shu-Kui; Kong Hong-Wei; Zhao Ming-Yue |
刊名 | acta chimica sinica
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出版日期 | 2006-09-28 |
卷号 | 64期号:18页码:1897-1903 |
关键词 | tobacco leaf organic alkaline compound comprehensive two dimensional gas chromatography (GC X GC) time of flight mass spectrometry (TOFMS) |
英文摘要 | comprehensive two-dimensional gas chromatography/time-of-flight mass spectrometry (gc x gc-tofms) has been applied for characterization of volatile and semi-volatile alkaline compounds in oriental tobacco leaf. simultaneous distillation extraction (sde) was used as the sample extraction method. two types of column set were compared, and appropriate gc x gc separation conditions were suggested. the results showed that the peaks detected by gc x gc method were far more than that by 1dgc. the separation behavior on 2d plot of different kinds of compounds was investigated. tofms library search combining structured chromatogram. of gc x gc was used to identify the nitrogen-containing compounds in tobacco leaf. a total of 92 alkaline compounds were tentatively identified. the results showed that gc x gc/tofms method is suitable for separation and identification of complex system. |
WOS标题词 | science & technology ; physical sciences |
类目[WOS] | chemistry, multidisciplinary |
研究领域[WOS] | chemistry |
关键词[WOS] | distillation-extraction ; complex samples ; pesticides ; gc |
收录类别 | SCI |
语种 | 英语 |
WOS记录号 | WOS:000241082000008 |
公开日期 | 2015-11-17 |
源URL | [http://159.226.238.44/handle/321008/139965] ![]() |
专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
作者单位 | 1.Changde Cigarette Factory, Ctr Sci & Technol, Changde 415000, Peoples R China 2.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatog R&A Ctr, Dalian 116023, Peoples R China 3.CNTC, Zhengzhou Tobacco Res Inst, Zhengzhou 450000, Peoples R China |
推荐引用方式 GB/T 7714 | Li Hai-Feng,Zhong Ke-Jun,Lu Xin,et al. Analysis of volatile and semi-volatile alkaline compounds in tobacco leaf by using comprehensive two-dimensional gas chromatography/time-of-flight mass spectrometry[J]. acta chimica sinica,2006,64(18):1897-1903. |
APA | Li Hai-Feng.,Zhong Ke-Jun.,Lu Xin.,Bai Chang-Min.,Huang Jian-Guo.,...&Xu Guo-Wang.(2006).Analysis of volatile and semi-volatile alkaline compounds in tobacco leaf by using comprehensive two-dimensional gas chromatography/time-of-flight mass spectrometry.acta chimica sinica,64(18),1897-1903. |
MLA | Li Hai-Feng,et al."Analysis of volatile and semi-volatile alkaline compounds in tobacco leaf by using comprehensive two-dimensional gas chromatography/time-of-flight mass spectrometry".acta chimica sinica 64.18(2006):1897-1903. |
入库方式: OAI收割
来源:大连化学物理研究所
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