Separation and identification of compounds in Adinandra nitida by comprehensive two-dimensional liquid chromatography coupled to atmospheric pressure chemical ionization source ion trap tandem mass spectrometry
文献类型:期刊论文
作者 | Zhang, Jie; Tao, Dingyin; Duan, Jicheng; Liang, Zhen; Zhang, Weibing; Zhang, Lihua; Huo, Yushu; Zhang, Yukui |
刊名 | analytical and bioanalytical chemistry
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出版日期 | 2006-10-01 |
卷号 | 386期号:3页码:586-593 |
关键词 | comprehensive two-dimensional liquid chromatography traditional Chinese medicine Adinandra nitida mass spectrometer monolithic column |
英文摘要 | a comprehensive two-dimensional liquid chromatographic (2d-lc) separation system based on the combination of a cn column and a merck chromolith flash reversed-phase column was developed for the separation of components in adinandra nitida, one type of traditional chinese medicine (tcm). the two dimensions were connected by a ten-port, dual-position valve controlled automatically by software written in-house. the effluents were detected by both ultraviolet and atmospheric pressure chemical ionization source ion trap tandem mass spectrometry (ms). the calculated peak capacity of the 2d-lc-ms/ms system was above 1240. more than 57 components were resolved in the methanol extract from adinandra nitida leaves, and five of these were identified based on their relative retention times, molecular weights and ms/ms spectra. |
WOS标题词 | science & technology ; life sciences & biomedicine ; physical sciences |
类目[WOS] | biochemical research methods ; chemistry, analytical |
研究领域[WOS] | biochemistry & molecular biology ; chemistry |
关键词[WOS] | traditional chinese medicines ; multidimensional separation ; stationary phases ; performance ; column ; resolution ; discovery ; mixtures ; proteins |
收录类别 | SCI |
语种 | 英语 |
WOS记录号 | WOS:000240713500020 |
公开日期 | 2015-11-17 |
源URL | [http://159.226.238.44/handle/321008/139990] ![]() |
专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
作者单位 | 1.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatogr Res & Anal Ctr, Dalian 116023, Peoples R China 2.Univ Texas, Hlth Sci Ctr, San Antonio, TX 78229 USA |
推荐引用方式 GB/T 7714 | Zhang, Jie,Tao, Dingyin,Duan, Jicheng,et al. Separation and identification of compounds in Adinandra nitida by comprehensive two-dimensional liquid chromatography coupled to atmospheric pressure chemical ionization source ion trap tandem mass spectrometry[J]. analytical and bioanalytical chemistry,2006,386(3):586-593. |
APA | Zhang, Jie.,Tao, Dingyin.,Duan, Jicheng.,Liang, Zhen.,Zhang, Weibing.,...&Zhang, Yukui.(2006).Separation and identification of compounds in Adinandra nitida by comprehensive two-dimensional liquid chromatography coupled to atmospheric pressure chemical ionization source ion trap tandem mass spectrometry.analytical and bioanalytical chemistry,386(3),586-593. |
MLA | Zhang, Jie,et al."Separation and identification of compounds in Adinandra nitida by comprehensive two-dimensional liquid chromatography coupled to atmospheric pressure chemical ionization source ion trap tandem mass spectrometry".analytical and bioanalytical chemistry 386.3(2006):586-593. |
入库方式: OAI收割
来源:大连化学物理研究所
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