中国科学院机构知识库网格
Chinese Academy of Sciences Institutional Repositories Grid
Simultaneous determination of polyphenols in tobacco by high performance liquid chromatography/photodiode array detection

文献类型:期刊论文

作者Bai Changmin; Zhong Kejun; Huang Jianguo; Cao Guojun; Xu Guowang
刊名chinese journal of analytical chemistry
出版日期2006-11-01
卷号34期号:11页码:1619-1621
关键词tobacco polyphenol ultrasonic extraction high performance liquid chromatography
英文摘要chlorogenic acid, chrysatropic acid and rutin in tobacco were analyzed using high performance liquid chromatography( hplc) /photodiode array deteciton (pda). after the tobacco was simply treated by ultrasonic extraction using methanol/water (4: 1, v/ v) and filtration, the obtained liquid sample was analyzed by hplc using hypersil ods column ( 4.6 mm x 150 min i. d., 3 mu m). methanol/trifluoroacetic acid (tfa) aqueous solution was used as mobile phase for gradient elution. pda spectrum was used for assistant identification. internal standard method was applied for quantitation. the recovery was in the range of 84.4% -96.4%. the relative standard deviation of determination was 1. 4% - 6. 4% for three compounds.
WOS标题词science & technology ; physical sciences
类目[WOS]chemistry, analytical
研究领域[WOS]chemistry
关键词[WOS]chlorogenic acid ; rutin ; separation ; cigarettes ; capillary
收录类别SCI
语种英语
WOS记录号WOS:000244672100024
公开日期2015-11-17
源URL[http://159.226.238.44/handle/321008/140029]  
专题大连化学物理研究所_中国科学院大连化学物理研究所
作者单位1.Changde Cigarette Factory, Ctr Sci & Technol, Changde 415000, Peoples R China
2.Chinese Acad Sci, Natl Chromatog Res & Anal Ctr, Dalian Inst Chem Phys, Dalian 116023, Peoples R China
3.Nanjing Univ Sci & Technol, Nanjing 210094, Peoples R China
推荐引用方式
GB/T 7714
Bai Changmin,Zhong Kejun,Huang Jianguo,et al. Simultaneous determination of polyphenols in tobacco by high performance liquid chromatography/photodiode array detection[J]. chinese journal of analytical chemistry,2006,34(11):1619-1621.
APA Bai Changmin,Zhong Kejun,Huang Jianguo,Cao Guojun,&Xu Guowang.(2006).Simultaneous determination of polyphenols in tobacco by high performance liquid chromatography/photodiode array detection.chinese journal of analytical chemistry,34(11),1619-1621.
MLA Bai Changmin,et al."Simultaneous determination of polyphenols in tobacco by high performance liquid chromatography/photodiode array detection".chinese journal of analytical chemistry 34.11(2006):1619-1621.

入库方式: OAI收割

来源:大连化学物理研究所

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