Simultaneous determination of polyphenols in tobacco by high performance liquid chromatography/photodiode array detection
文献类型:期刊论文
作者 | Bai Changmin; Zhong Kejun; Huang Jianguo; Cao Guojun; Xu Guowang |
刊名 | chinese journal of analytical chemistry
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出版日期 | 2006-11-01 |
卷号 | 34期号:11页码:1619-1621 |
关键词 | tobacco polyphenol ultrasonic extraction high performance liquid chromatography |
英文摘要 | chlorogenic acid, chrysatropic acid and rutin in tobacco were analyzed using high performance liquid chromatography( hplc) /photodiode array deteciton (pda). after the tobacco was simply treated by ultrasonic extraction using methanol/water (4: 1, v/ v) and filtration, the obtained liquid sample was analyzed by hplc using hypersil ods column ( 4.6 mm x 150 min i. d., 3 mu m). methanol/trifluoroacetic acid (tfa) aqueous solution was used as mobile phase for gradient elution. pda spectrum was used for assistant identification. internal standard method was applied for quantitation. the recovery was in the range of 84.4% -96.4%. the relative standard deviation of determination was 1. 4% - 6. 4% for three compounds. |
WOS标题词 | science & technology ; physical sciences |
类目[WOS] | chemistry, analytical |
研究领域[WOS] | chemistry |
关键词[WOS] | chlorogenic acid ; rutin ; separation ; cigarettes ; capillary |
收录类别 | SCI |
语种 | 英语 |
WOS记录号 | WOS:000244672100024 |
公开日期 | 2015-11-17 |
源URL | [http://159.226.238.44/handle/321008/140029] ![]() |
专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
作者单位 | 1.Changde Cigarette Factory, Ctr Sci & Technol, Changde 415000, Peoples R China 2.Chinese Acad Sci, Natl Chromatog Res & Anal Ctr, Dalian Inst Chem Phys, Dalian 116023, Peoples R China 3.Nanjing Univ Sci & Technol, Nanjing 210094, Peoples R China |
推荐引用方式 GB/T 7714 | Bai Changmin,Zhong Kejun,Huang Jianguo,et al. Simultaneous determination of polyphenols in tobacco by high performance liquid chromatography/photodiode array detection[J]. chinese journal of analytical chemistry,2006,34(11):1619-1621. |
APA | Bai Changmin,Zhong Kejun,Huang Jianguo,Cao Guojun,&Xu Guowang.(2006).Simultaneous determination of polyphenols in tobacco by high performance liquid chromatography/photodiode array detection.chinese journal of analytical chemistry,34(11),1619-1621. |
MLA | Bai Changmin,et al."Simultaneous determination of polyphenols in tobacco by high performance liquid chromatography/photodiode array detection".chinese journal of analytical chemistry 34.11(2006):1619-1621. |
入库方式: OAI收割
来源:大连化学物理研究所
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