Establishment and application of on-line parallel-trap SFE-HPLC system
文献类型:期刊论文
作者 | Zhang Jie; Liang Zhen; Zhang Li-Hua; Zhang Wei-Bing; Huo Yu-Shu; Zhang Yu-Kui |
刊名 | chemical journal of chinese universities-chinese |
出版日期 | 2006-12-10 |
卷号 | 27期号:12页码:2291-2293 |
关键词 | supercritical fluid extraction high performance liquid chromatography Ganoderma lucidum |
英文摘要 | a novel on-line parallel-trap supercritical fluid extraction (sfe)-high performance liquid chromatography (hplc) system was established. the interfere consisted of automated ten-port valve and parallel traps were used to carry out continuous and alternate trapping and transferring of the sample extracted with supercritical carbon dioxide, and hplc was used to analyze the transfer-red sample. the novel on-line system was used to monitor the extraction process of fruiting bodies of ganoderma lucidum. the extracts of six consecutive cycles were analyzed and the optimum extraction time was determined, which accorded with the result obtained with off-line extraction. using this system, the whole process can be monitored and the optimum extraction time can be determined with single run. in addition, it has many other advantages, such as low sample loading, high sensitivity and accuracy, short analysis time, avoiding sample pollution and easily operation etc. the system shows a great potential in the extraction and analysis of the complicated samples including traditional chinese medicine and environmental samples etc. |
WOS标题词 | science & technology ; physical sciences |
类目[WOS] | chemistry, multidisciplinary |
研究领域[WOS] | chemistry |
关键词[WOS] | supercritical-fluid extraction ; chromatography-mass spectrometry ; liquid-chromatography ; aromatic-hydrocarbons |
收录类别 | SCI |
语种 | 英语 |
WOS记录号 | WOS:000242962700012 |
公开日期 | 2015-11-17 |
源URL | [http://159.226.238.44/handle/321008/140223] |
专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
作者单位 | 1.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatog R&A Ctr, Dalian 116023, Peoples R China 2.Univ Texas, Hlth Sci Ctr, San Antonio, TX 78229 USA |
推荐引用方式 GB/T 7714 | Zhang Jie,Liang Zhen,Zhang Li-Hua,et al. Establishment and application of on-line parallel-trap SFE-HPLC system[J]. chemical journal of chinese universities-chinese,2006,27(12):2291-2293. |
APA | Zhang Jie,Liang Zhen,Zhang Li-Hua,Zhang Wei-Bing,Huo Yu-Shu,&Zhang Yu-Kui.(2006).Establishment and application of on-line parallel-trap SFE-HPLC system.chemical journal of chinese universities-chinese,27(12),2291-2293. |
MLA | Zhang Jie,et al."Establishment and application of on-line parallel-trap SFE-HPLC system".chemical journal of chinese universities-chinese 27.12(2006):2291-2293. |
入库方式: OAI收割
来源:大连化学物理研究所
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