Separation of D-amino acids by capillary electrophoresis using P-aectamidobenzenesulfonyl fluoride as derivatization reagent
文献类型：期刊论文
| 作者 | Qu Qishu; Tang Xiaoqing; Wang Chengyin; Yang Gongjun; Hu Xiaoya; Zhang Yukui; Yan Chao |
| 刊名 | chinese journal of analytical chemistry
 |
| 出版日期 | 2006-11-01 |
| 卷号 | 34期号:11页码:1587-1590 |
| 关键词 | capillary electrophoresis D-amino acid derivatization |
| 英文摘要 | a new method for the separation of 19 standard d-amino acids and glycine ( gly) by capillary electrophoresis ( ce) using p-acetamidobenzenesulfonyl fluoride ( paabs-f) as precolumn derivatization reagent has been developed. the separation conditions were carefully studied and optimized. the experimental results showed that 20 mmmol/l sodium borate ( ph 9.3), 126 mmmol/l sodium dodecyl sulfate, 8 mmol/l,8-cyclodextrin and 20 mmol/l nacl were the optimal conditions for the ce separation. under the optimal conditions, 19 stangdard d-amino acids and gly were successfully achied with baseline separation within 16 min by ce. |
| WOS标题词 | science & technology ; physical sciences |
| 类目[WOS] | chemistry, analytical |
| 研究领域[WOS] | chemistry |
| 关键词[WOS] | chromatography |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000244672100016 |
| 公开日期 | 2015-11-17 |
| 源URL | [http://159.226.238.44/handle/321008/140251]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | 1.Yangzhou Univ, Jiangsu Key Lab Environm Mat & Environm Engn, Coll Chem & Chem Engn, Yangzhou 225002, Peoples R China 2.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatog Res & Anal Ctr, Dalian 116011, Peoples R China |
| 推荐引用方式 GB/T 7714 | Qu Qishu,Tang Xiaoqing,Wang Chengyin,et al. Separation of D-amino acids by capillary electrophoresis using P-aectamidobenzenesulfonyl fluoride as derivatization reagent[J]. chinese journal of analytical chemistry,2006,34(11):1587-1590. |
| APA | Qu Qishu.,Tang Xiaoqing.,Wang Chengyin.,Yang Gongjun.,Hu Xiaoya.,...&Yan Chao.(2006).Separation of D-amino acids by capillary electrophoresis using P-aectamidobenzenesulfonyl fluoride as derivatization reagent.chinese journal of analytical chemistry,34(11),1587-1590. |
| MLA | Qu Qishu,et al."Separation of D-amino acids by capillary electrophoresis using P-aectamidobenzenesulfonyl fluoride as derivatization reagent".chinese journal of analytical chemistry 34.11(2006):1587-1590. |
入库方式： OAI收割
来源：大连化学物理研究所
浏览0
下载0
收藏0
其他版本
除非特别说明，本系统中所有内容都受版权保护，并保留所有权利。