Determination of the monomers in phenylethylene-butyl acrylate-vinyl triethoxy siloxane terpolymer for solid phase microextraction coating by combining IR and UV
文献类型：期刊论文
| 作者 | Shen Shu-chang; Liu Cai-yun; Fu Shuang; Zhang Wei-bing; Wang Wen-bo |
| 刊名 | spectroscopy and spectral analysis
 |
| 出版日期 | 2007-11-01 |
| 卷号 | 27期号:11页码:2235-2238 |
| 关键词 | solid phase microextraction coating Phenylethylene-butyl acrylate-vinyl triethoxy siloxane terpolymer Combining RI and UV Monomer content |
| 英文摘要 | in the present paper, phenylethylene-butyl acrylate-vinyl triethoxy siloxane terpolymer, as spme coating, was synthesized. combining infrared spectrum and ultraviolet spectrum, the contents of the monomers were determined. the two monomers' mole ratio of phenylethylene to butyl acrylate was obtained by ir the content of phenylethylene was obtained by uv. then the contents of butyl acrylate and vinyl triethoxy siloxane were calculated from the phenylethylene quantity and the mole ratio. for the determination of the mole ratio of phenylethylene to butyl acrylate, the standard curve was a(r) =0.114m, +0. 032 (a: absorptance ratio, mn,: mole ratio), and the correlation efficient(r(2)) was 0. 999 3; for the determination of the content of phenylethylene, the standard curve was delta a=0.078 6c+0.081 2(delta a: absorptance difference, c: concentration of phenylethylene), and the correlation efficient(r(2)) was 0. 998 9. the relative standard deviation (rsd) for phenylethylene was 0. 41%, and recoveries were 97. 8%-104%. the relative standard deviation (rsd) for butyl acrylate was 0. 39%, and the recoveries were 97. 1%-99. 6%. |
| WOS标题词 | science & technology ; technology |
| 类目[WOS] | spectroscopy |
| 研究领域[WOS] | spectroscopy |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000251431300023 |
| 公开日期 | 2015-11-17 |
| 源URL | [http://159.226.238.44/handle/321008/140525]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | 1.Qiqihar Univ, Coll Chem & Chem Engn, Qiqihar 161006, Peoples R China 2.Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116011, Peoples R China |
| 推荐引用方式 GB/T 7714 | Shen Shu-chang,Liu Cai-yun,Fu Shuang,et al. Determination of the monomers in phenylethylene-butyl acrylate-vinyl triethoxy siloxane terpolymer for solid phase microextraction coating by combining IR and UV[J]. spectroscopy and spectral analysis,2007,27(11):2235-2238. |
| APA | Shen Shu-chang,Liu Cai-yun,Fu Shuang,Zhang Wei-bing,&Wang Wen-bo.(2007).Determination of the monomers in phenylethylene-butyl acrylate-vinyl triethoxy siloxane terpolymer for solid phase microextraction coating by combining IR and UV.spectroscopy and spectral analysis,27(11),2235-2238. |
| MLA | Shen Shu-chang,et al."Determination of the monomers in phenylethylene-butyl acrylate-vinyl triethoxy siloxane terpolymer for solid phase microextraction coating by combining IR and UV".spectroscopy and spectral analysis 27.11(2007):2235-2238. |
入库方式： OAI收割
来源：大连化学物理研究所
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