The covalently bonded cellulose tris(3,5-dimethylphenylcarbamate) on a silica monolithic capillary column for enantioseparation in capillary electrochromatography
文献类型:期刊论文
作者 | Dong, Xiaoli1,2; Wu, Ren'an1; Dong, Jing1; Wu, Minghuo1; Zhu, Yan2; Zou, Hanfa1 |
刊名 | journal of chromatography b-analytical technologies in the biomedical and life sciences
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出版日期 | 2008-11-01 |
卷号 | 875期号:1页码:317-322 |
关键词 | Capillary electrochromatography Cellulose tris(3 Covalently bonded chiral stationary phase Enantioseparation Silica monolithic column 5-dimethylphenylcarbamate) |
英文摘要 | a chiral capillary monolithic column for capillary electrochromatography (cec) was prepared by covalent bonding of cellulose tris(3,5-dimethylphenylcarbamate) (cdmpc) on the silica monolithic matrix within the confine of a 50-mu m i.d. bare fused silica capillary. several pairs of enantiomers including neutral and basic analytes were baseline resolved on the newly prepared chiral capillary monolithic column in cec with aqueous mobile phases. fast enantioseparation was achieved due to the favorable dynamic properties of silica monolith. the covalent bonding of cdmpc as the chiral stationary phase for cec also enabled the use of thf in mobile phase for enantioseparation of prazquantel by overcoming the incompatibility of thf and the physically coated cdmpc on a column. (c) 2008 published by elsevier b.v. |
WOS标题词 | science & technology ; life sciences & biomedicine ; physical sciences |
类目[WOS] | biochemical research methods ; chemistry, analytical |
研究领域[WOS] | biochemistry & molecular biology ; chemistry |
关键词[WOS] | chiral stationary-phase ; liquid-chromatographic enantioseparations ; charged polyacrylamide-gels ; enantiomeric separations ; polysaccharide derivatives ; vancomycin ; tris(3,5-dichlorophenylcarbamate) ; size |
收录类别 | SCI |
语种 | 英语 |
WOS记录号 | WOS:000260945800042 |
公开日期 | 2015-11-17 |
源URL | [http://159.226.238.44/handle/321008/140808] ![]() |
专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
作者单位 | 1.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatograph R&A Ctr, Dalian 116023, Peoples R China 2.Zhejiang Univ, Dept Chem, Hangzhou 310028, Peoples R China |
推荐引用方式 GB/T 7714 | Dong, Xiaoli,Wu, Ren'an,Dong, Jing,et al. The covalently bonded cellulose tris(3,5-dimethylphenylcarbamate) on a silica monolithic capillary column for enantioseparation in capillary electrochromatography[J]. journal of chromatography b-analytical technologies in the biomedical and life sciences,2008,875(1):317-322. |
APA | Dong, Xiaoli,Wu, Ren'an,Dong, Jing,Wu, Minghuo,Zhu, Yan,&Zou, Hanfa.(2008).The covalently bonded cellulose tris(3,5-dimethylphenylcarbamate) on a silica monolithic capillary column for enantioseparation in capillary electrochromatography.journal of chromatography b-analytical technologies in the biomedical and life sciences,875(1),317-322. |
MLA | Dong, Xiaoli,et al."The covalently bonded cellulose tris(3,5-dimethylphenylcarbamate) on a silica monolithic capillary column for enantioseparation in capillary electrochromatography".journal of chromatography b-analytical technologies in the biomedical and life sciences 875.1(2008):317-322. |
入库方式: OAI收割
来源:大连化学物理研究所
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