中国科学院机构知识库网格
Chinese Academy of Sciences Institutional Repositories Grid
The covalently bonded cellulose tris(3,5-dimethylphenylcarbamate) on a silica monolithic capillary column for enantioseparation in capillary electrochromatography

文献类型:期刊论文

作者Dong, Xiaoli1,2; Wu, Ren'an1; Dong, Jing1; Wu, Minghuo1; Zhu, Yan2; Zou, Hanfa1
刊名journal of chromatography b-analytical technologies in the biomedical and life sciences
出版日期2008-11-01
卷号875期号:1页码:317-322
关键词Capillary electrochromatography Cellulose tris(3 Covalently bonded chiral stationary phase Enantioseparation Silica monolithic column 5-dimethylphenylcarbamate)
英文摘要a chiral capillary monolithic column for capillary electrochromatography (cec) was prepared by covalent bonding of cellulose tris(3,5-dimethylphenylcarbamate) (cdmpc) on the silica monolithic matrix within the confine of a 50-mu m i.d. bare fused silica capillary. several pairs of enantiomers including neutral and basic analytes were baseline resolved on the newly prepared chiral capillary monolithic column in cec with aqueous mobile phases. fast enantioseparation was achieved due to the favorable dynamic properties of silica monolith. the covalent bonding of cdmpc as the chiral stationary phase for cec also enabled the use of thf in mobile phase for enantioseparation of prazquantel by overcoming the incompatibility of thf and the physically coated cdmpc on a column. (c) 2008 published by elsevier b.v.
WOS标题词science & technology ; life sciences & biomedicine ; physical sciences
类目[WOS]biochemical research methods ; chemistry, analytical
研究领域[WOS]biochemistry & molecular biology ; chemistry
关键词[WOS]chiral stationary-phase ; liquid-chromatographic enantioseparations ; charged polyacrylamide-gels ; enantiomeric separations ; polysaccharide derivatives ; vancomycin ; tris(3,5-dichlorophenylcarbamate) ; size
收录类别SCI
语种英语
WOS记录号WOS:000260945800042
公开日期2015-11-17
源URL[http://159.226.238.44/handle/321008/140808]  
专题大连化学物理研究所_中国科学院大连化学物理研究所
作者单位1.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatograph R&A Ctr, Dalian 116023, Peoples R China
2.Zhejiang Univ, Dept Chem, Hangzhou 310028, Peoples R China
推荐引用方式
GB/T 7714
Dong, Xiaoli,Wu, Ren'an,Dong, Jing,et al. The covalently bonded cellulose tris(3,5-dimethylphenylcarbamate) on a silica monolithic capillary column for enantioseparation in capillary electrochromatography[J]. journal of chromatography b-analytical technologies in the biomedical and life sciences,2008,875(1):317-322.
APA Dong, Xiaoli,Wu, Ren'an,Dong, Jing,Wu, Minghuo,Zhu, Yan,&Zou, Hanfa.(2008).The covalently bonded cellulose tris(3,5-dimethylphenylcarbamate) on a silica monolithic capillary column for enantioseparation in capillary electrochromatography.journal of chromatography b-analytical technologies in the biomedical and life sciences,875(1),317-322.
MLA Dong, Xiaoli,et al."The covalently bonded cellulose tris(3,5-dimethylphenylcarbamate) on a silica monolithic capillary column for enantioseparation in capillary electrochromatography".journal of chromatography b-analytical technologies in the biomedical and life sciences 875.1(2008):317-322.

入库方式: OAI收割

来源:大连化学物理研究所

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