"Click oligo(ethylene glycol)": An excellent orthogonal stationary phase to C18 for two-dimensional reversed-phase/reversed-phase liquid chromatography
文献类型：期刊论文
| 作者 | Liu, Yanming; Guo, Zhimou; Jin, Yu; Xue, Xingya; Xu, Qing; Zhang, Feifang; Liang, Xinmiao |
| 刊名 | journal of chromatography a
 |
| 出版日期 | 2008-10-10 |
| 卷号 | 1206期号:2页码:153-159 |
| 关键词 | Click OEG stationary phase oligo(ethylene glycol) orthogonality RP/RP two-dimensional liquid chromatography traditional Chinese medicine |
| 英文摘要 | a novel click oligo(ethylene glycol) (click oeg) stationary phase was proposed for constructing two-dimensional reversed-phase/reversed-phase liquid chromatography system (2d-rp/rplc) combined with c18. the new stationary phase was prepared by immobilization of oligo(ethylene glycol) on silica support via click chemistry. and the resulting material was characterized by ft-ir, solid state cp/mas c-13 nmr and elemental analysis. the investigation on orthogonality between click oeg and c18 was performed by geometric approach with a set of testsolutes. the orthogonality reached 68.94%, which is much higher than other combinations. an offline 2dlc system consisted of click oeg and c18 was constructed and applied to the analysis of a kind of traditional chinese medicine lignum dalbergiae odoriferae. excellent separation results validated the high orthogonality between the click oeg and c18 in the practical separation of complex samples. (c) 2008 elsevier b.v. all rights reserved. |
| WOS标题词 | science & technology ; life sciences & biomedicine ; physical sciences |
| 类目[WOS] | biochemical research methods ; chemistry, analytical |
| 研究领域[WOS] | biochemistry & molecular biology ; chemistry |
| 关键词[WOS] | self-assembled monolayers ; proteomic samples ; peak-capacity ; off-line ; separation ; performance ; silica ; hplc ; resolution ; chemistry |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000259944000009 |
| 公开日期 | 2015-11-17 |
| 源URL | [http://159.226.238.44/handle/321008/140966]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116023, Liaoning, Peoples R China |
| 推荐引用方式 GB/T 7714 | Liu, Yanming,Guo, Zhimou,Jin, Yu,et al. "Click oligo(ethylene glycol)": An excellent orthogonal stationary phase to C18 for two-dimensional reversed-phase/reversed-phase liquid chromatography[J]. journal of chromatography a,2008,1206(2):153-159. |
| APA | Liu, Yanming.,Guo, Zhimou.,Jin, Yu.,Xue, Xingya.,Xu, Qing.,...&Liang, Xinmiao.(2008)."Click oligo(ethylene glycol)": An excellent orthogonal stationary phase to C18 for two-dimensional reversed-phase/reversed-phase liquid chromatography.journal of chromatography a,1206(2),153-159. |
| MLA | Liu, Yanming,et al.""Click oligo(ethylene glycol)": An excellent orthogonal stationary phase to C18 for two-dimensional reversed-phase/reversed-phase liquid chromatography".journal of chromatography a 1206.2(2008):153-159. |
入库方式： OAI收割
来源：大连化学物理研究所
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