Analysis of alkylbenzene samples by comprehensive capillary liquid chromatography x capillary gas chromatography
文献类型：期刊论文
| 作者 | Xu, Yuan; Wang, Hua; Zhao, Jinghong; Guan, Yafeng |
| 刊名 | journal of chromatography a
 |
| 出版日期 | 2008-02-15 |
| 卷号 | 1181期号:1-2页码:95-102 |
| 关键词 | on-line-coupled micro-LC-GC comprehensive LC x GC group-type separation heavy alkylbenzene |
| 英文摘要 | the constituents in synthetic alkylbenzene samples were analyzed by a comprehensive capillary liquid chromatography ( mu-lc) x capillary gas chromatography (cgc). the mu-lc separates the mixture into aliphatic compounds, monosubstituted alkylbenzenes, multi substituted alkylbenzenes and binuclear aromatic compounds. each fraction from a single mu-lc injection is stored in turn in a multiloop interface, and then transferred online into cgc sequentially with large volume in-column splitless injection technique for detailed analysis. no sample discrimination was found with this coupling and injection technique. both the mu-lc column dimension and transfer speed of fraction from interface to cgc were optimized. quantitative results and the carbon number distribution of each chemical class are obtained by using the comprehensive mu-lc x cgc with flame ionization detection. the reproducibility of peak area is better than 2% rsd. (c) 2007 elsevier b.v. all rights reserved. |
| WOS标题词 | science & technology ; life sciences & biomedicine ; physical sciences |
| 类目[WOS] | biochemical research methods ; chemistry, analytical |
| 研究领域[WOS] | biochemistry & molecular biology ; chemistry |
| 关键词[WOS] | mass-spectrometry ; supercritical-fluid ; micro hplc ; lc ; gc ; identification ; extraction ; column ; oil ; ms |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000253506600011 |
| 公开日期 | 2015-11-17 |
| 源URL | [http://159.226.238.44/handle/321008/141015]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116023, Peoples R China |
| 推荐引用方式 GB/T 7714 | Xu, Yuan,Wang, Hua,Zhao, Jinghong,et al. Analysis of alkylbenzene samples by comprehensive capillary liquid chromatography x capillary gas chromatography[J]. journal of chromatography a,2008,1181(1-2):95-102. |
| APA | Xu, Yuan,Wang, Hua,Zhao, Jinghong,&Guan, Yafeng.(2008).Analysis of alkylbenzene samples by comprehensive capillary liquid chromatography x capillary gas chromatography.journal of chromatography a,1181(1-2),95-102. |
| MLA | Xu, Yuan,et al."Analysis of alkylbenzene samples by comprehensive capillary liquid chromatography x capillary gas chromatography".journal of chromatography a 1181.1-2(2008):95-102. |
入库方式： OAI收割
来源：大连化学物理研究所
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