Thermal stability, decomposition and glass transition behavior of PANI/NiO composites
文献类型：期刊论文
| 作者 | Qi, Yanni1; Zhang, Jian1; Qiu, Shujun1; Sun, Lixian1; Xu, Fen2; Zhu, Min3; Ouyang, Liuzhang3; Sun, Dalin4 |
| 刊名 | journal of thermal analysis and calorimetry
 |
| 出版日期 | 2009-11-01 |
| 卷号 | 98期号:2页码:533-537 |
| 关键词 | PANI/NiO composite Thermal stability TG-MS analysis T-g |
| 英文摘要 | polyaniline/nio (pani/nio) composites were synthesized by in situ polymerization at the presence of hcl (as dopant). ftir, tem and xrd were used to characterize the composites. thermogravimetry (tg)-mass spectrometer (ms) and temperature modulated differential scanning calorimetry (tmdsc) were used to study the thermal stability, decomposition and glass transition temperature (t (g)) of the composites, respectively. ftir and xrd results showed that nio nanoparticles connected with pani chains in the pani/nio composites. tem results exhibited that the morphologies of pani/nio composites were mostly spherical, which were different from the wirelike pani. tg-ms curves indicated that the products for oxidative degradation of both pani and pani/nio composite were h2o, co2, no and no2. tg curves showed that with nio contents increased in pani/nio composites, thermal stability of pani/nio composites increased firstly and then decreased when the nio content was higher than 66.2 wt%. t (g) of pani/nio composites also increased from 163.19 to 252.36 a degrees c with nio content increasing from 0 to 50 wt%, and then decreased with nio content increasing continuously. |
| WOS标题词 | science & technology ; physical sciences |
| 类目[WOS] | chemistry, analytical ; chemistry, physical |
| 研究领域[WOS] | chemistry |
| 关键词[WOS] | tg-ms analysis ; polyaniline ; nanoparticles ; nanocomposites ; degradation ; polymers |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000271108500026 |
| 公开日期 | 2015-11-17 |
| 源URL | [http://159.226.238.44/handle/321008/141611]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | 1.Chinese Acad Sci, Dalian Inst Chem Phys, Mat & Thermochem Lab, Dalian 116023, Peoples R China 2.Liaoning Normal Univ, Fac Chem & Chem Engn, Dalian 116023, Peoples R China 3.S China Univ Technol, Sch Mat Sci & Engn, Guangzhou 510640, Guangdong, Peoples R China 4.Fudan Univ, Dept Mat Sci, Shanghai 200433, Peoples R China |
| 推荐引用方式 GB/T 7714 | Qi, Yanni,Zhang, Jian,Qiu, Shujun,et al. Thermal stability, decomposition and glass transition behavior of PANI/NiO composites[J]. journal of thermal analysis and calorimetry,2009,98(2):533-537. |
| APA | Qi, Yanni.,Zhang, Jian.,Qiu, Shujun.,Sun, Lixian.,Xu, Fen.,...&Sun, Dalin.(2009).Thermal stability, decomposition and glass transition behavior of PANI/NiO composites.journal of thermal analysis and calorimetry,98(2),533-537. |
| MLA | Qi, Yanni,et al."Thermal stability, decomposition and glass transition behavior of PANI/NiO composites".journal of thermal analysis and calorimetry 98.2(2009):533-537. |
入库方式： OAI收割
来源：大连化学物理研究所
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