Separation and detection of polar cuticular components from Oriental tobacco leaf by integration of normal-phase liquid chromatography fractionation with reversed-phase liquid chromatography-mass spectrometry
文献类型:期刊论文
作者 | Ding, Li1; Xie, Fuwei1; Xu, Guowang2; Liu, Kejian1; Wang, Sheng1; Xie, Jianping1 |
刊名 | journal of separation science
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出版日期 | 2010-11-01 |
卷号 | 33期号:21页码:3429-3436 |
关键词 | ESI/MS Normal-phase LC RPLC Tobacco cuticular components |
英文摘要 | integration of normal-phase lc (nplc) fractionation with rplc-esi/ms was established to detect the polar fractions of cuticular components from oriental tobacco leaf. nplc was selected for the fractionation of polar components of cuticular leaf extract, after being concentrated with rotary evaporator, each of the enriched fractions was further analyzed by rplc-esi/ms. in total, 83 compounds were finally detected including 45 cembranoids, 15 labdanoids, 20 sucrose esters, and 3 glucose esters (or fructose esters). three cembranoids and seven labdanoids possibly are new diterpenoids. glucose esters (or fructose esters) are also reported in nicotiana tobacco for the first time. |
WOS标题词 | science & technology ; physical sciences |
类目[WOS] | chemistry, analytical |
研究领域[WOS] | chemistry |
关键词[WOS] | 2-dimensional gas-chromatography ; traditional chinese medicines ; sucrose esters ; ion-exchange ; macrocyclic diterpenes ; labdanic compounds ; greek tobacco ; chemistry ; volatile ; cembratrienetriols |
收录类别 | SCI |
语种 | 英语 |
WOS记录号 | WOS:000284230700020 |
公开日期 | 2015-11-17 |
源URL | [http://159.226.238.44/handle/321008/141673] ![]() |
专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
作者单位 | 1.Zhengzhou Tobacco Res Inst CNTC, Key Lab Tobacco Chem, Zhengzhou 450001, Peoples R China 2.Chinese Acad Sci, Dalian Inst Chem Phys, CAS Key Lab Separat Sci Analyt Chem, Dalian, Peoples R China |
推荐引用方式 GB/T 7714 | Ding, Li,Xie, Fuwei,Xu, Guowang,et al. Separation and detection of polar cuticular components from Oriental tobacco leaf by integration of normal-phase liquid chromatography fractionation with reversed-phase liquid chromatography-mass spectrometry[J]. journal of separation science,2010,33(21):3429-3436. |
APA | Ding, Li,Xie, Fuwei,Xu, Guowang,Liu, Kejian,Wang, Sheng,&Xie, Jianping.(2010).Separation and detection of polar cuticular components from Oriental tobacco leaf by integration of normal-phase liquid chromatography fractionation with reversed-phase liquid chromatography-mass spectrometry.journal of separation science,33(21),3429-3436. |
MLA | Ding, Li,et al."Separation and detection of polar cuticular components from Oriental tobacco leaf by integration of normal-phase liquid chromatography fractionation with reversed-phase liquid chromatography-mass spectrometry".journal of separation science 33.21(2010):3429-3436. |
入库方式: OAI收割
来源:大连化学物理研究所
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