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Identification of prenyl flavonoid glycosides and phenolic acids in Epimedium koreanum Nakai by Q-TOF-MS combined with selective enrichment on "click oligo (ethylene glycol)" column

文献类型:期刊论文

作者Wang, Yaqin1,2; Guo, Zhimou1; Jin, Yu3; Zhang, Xiuli1; Wang, Li1; Xue, Xingya1; Liang, Xinmiao1
刊名journal of pharmaceutical and biomedical analysis
出版日期2010-02-05
卷号51期号:3页码:606-616
关键词Q-TOF-MS Prenyl flavonoid glycosides Phenolic acids Selective enrichment "Click oligo (ethylene glycol)" Epimedium koreanum Nakai
英文摘要prenyl flavonoid glycosides and phenolic acids are constituents of the medicinal plant epimedium koreanum nakai (ek). an efficient method was developed to enrich these compounds and identify them, using ultra performance liquid chromatography combined with q-tof-ms, and a "click oligo (ethylene glycol)" (click oeg) column. using this method, 51 prenyl flavonoid glycosides and 18 phenolic acids were identified or tentatively identified. of these, 11 prenyl flavonoid glycosides and 4 phenolic acids were new compounds, and 7 phenolic acids were newly identified in ek. therefore, ms combined with selective enrichment provided a powerful means for analyzing prenyl flavonoid glycosides and phenolic acids. (c) 2009 elsevier b.v. all rights reserved.
WOS标题词science & technology ; physical sciences ; life sciences & biomedicine
类目[WOS]chemistry, analytical ; pharmacology & pharmacy
研究领域[WOS]chemistry ; pharmacology & pharmacy
关键词[WOS]performance liquid-chromatography ; chlorogenic acids ; lc-msn ; oligo(ethylene glycol) ; mass-spectrometry ; stationary-phase ; dietary burden ; extraction ; separation ; isomers
收录类别SCI
语种英语
WOS记录号WOS:000272025800015
公开日期2015-11-17
源URL[http://159.226.238.44/handle/321008/141925]  
专题大连化学物理研究所_中国科学院大连化学物理研究所
作者单位1.Chinese Acad Sci, Key Lab Separat Sci Analyt Chem, Dalian 116023, Peoples R China
2.Shenyang Ligong Univ, Sch Environm & Chem Engn, Shenyang 110168, Peoples R China
3.E China Univ Sci & Technol, Sch Pharm, Shanghai 200237, Peoples R China
推荐引用方式
GB/T 7714
Wang, Yaqin,Guo, Zhimou,Jin, Yu,et al. Identification of prenyl flavonoid glycosides and phenolic acids in Epimedium koreanum Nakai by Q-TOF-MS combined with selective enrichment on "click oligo (ethylene glycol)" column[J]. journal of pharmaceutical and biomedical analysis,2010,51(3):606-616.
APA Wang, Yaqin.,Guo, Zhimou.,Jin, Yu.,Zhang, Xiuli.,Wang, Li.,...&Liang, Xinmiao.(2010).Identification of prenyl flavonoid glycosides and phenolic acids in Epimedium koreanum Nakai by Q-TOF-MS combined with selective enrichment on "click oligo (ethylene glycol)" column.journal of pharmaceutical and biomedical analysis,51(3),606-616.
MLA Wang, Yaqin,et al."Identification of prenyl flavonoid glycosides and phenolic acids in Epimedium koreanum Nakai by Q-TOF-MS combined with selective enrichment on "click oligo (ethylene glycol)" column".journal of pharmaceutical and biomedical analysis 51.3(2010):606-616.

入库方式: OAI收割

来源:大连化学物理研究所

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