Identification of prenyl flavonoid glycosides and phenolic acids in Epimedium koreanum Nakai by Q-TOF-MS combined with selective enrichment on "click oligo (ethylene glycol)" column
文献类型:期刊论文
作者 | Wang, Yaqin1,2; Guo, Zhimou1; Jin, Yu3; Zhang, Xiuli1; Wang, Li1; Xue, Xingya1; Liang, Xinmiao1 |
刊名 | journal of pharmaceutical and biomedical analysis
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出版日期 | 2010-02-05 |
卷号 | 51期号:3页码:606-616 |
关键词 | Q-TOF-MS Prenyl flavonoid glycosides Phenolic acids Selective enrichment "Click oligo (ethylene glycol)" Epimedium koreanum Nakai |
英文摘要 | prenyl flavonoid glycosides and phenolic acids are constituents of the medicinal plant epimedium koreanum nakai (ek). an efficient method was developed to enrich these compounds and identify them, using ultra performance liquid chromatography combined with q-tof-ms, and a "click oligo (ethylene glycol)" (click oeg) column. using this method, 51 prenyl flavonoid glycosides and 18 phenolic acids were identified or tentatively identified. of these, 11 prenyl flavonoid glycosides and 4 phenolic acids were new compounds, and 7 phenolic acids were newly identified in ek. therefore, ms combined with selective enrichment provided a powerful means for analyzing prenyl flavonoid glycosides and phenolic acids. (c) 2009 elsevier b.v. all rights reserved. |
WOS标题词 | science & technology ; physical sciences ; life sciences & biomedicine |
类目[WOS] | chemistry, analytical ; pharmacology & pharmacy |
研究领域[WOS] | chemistry ; pharmacology & pharmacy |
关键词[WOS] | performance liquid-chromatography ; chlorogenic acids ; lc-msn ; oligo(ethylene glycol) ; mass-spectrometry ; stationary-phase ; dietary burden ; extraction ; separation ; isomers |
收录类别 | SCI |
语种 | 英语 |
WOS记录号 | WOS:000272025800015 |
公开日期 | 2015-11-17 |
源URL | [http://159.226.238.44/handle/321008/141925] ![]() |
专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
作者单位 | 1.Chinese Acad Sci, Key Lab Separat Sci Analyt Chem, Dalian 116023, Peoples R China 2.Shenyang Ligong Univ, Sch Environm & Chem Engn, Shenyang 110168, Peoples R China 3.E China Univ Sci & Technol, Sch Pharm, Shanghai 200237, Peoples R China |
推荐引用方式 GB/T 7714 | Wang, Yaqin,Guo, Zhimou,Jin, Yu,et al. Identification of prenyl flavonoid glycosides and phenolic acids in Epimedium koreanum Nakai by Q-TOF-MS combined with selective enrichment on "click oligo (ethylene glycol)" column[J]. journal of pharmaceutical and biomedical analysis,2010,51(3):606-616. |
APA | Wang, Yaqin.,Guo, Zhimou.,Jin, Yu.,Zhang, Xiuli.,Wang, Li.,...&Liang, Xinmiao.(2010).Identification of prenyl flavonoid glycosides and phenolic acids in Epimedium koreanum Nakai by Q-TOF-MS combined with selective enrichment on "click oligo (ethylene glycol)" column.journal of pharmaceutical and biomedical analysis,51(3),606-616. |
MLA | Wang, Yaqin,et al."Identification of prenyl flavonoid glycosides and phenolic acids in Epimedium koreanum Nakai by Q-TOF-MS combined with selective enrichment on "click oligo (ethylene glycol)" column".journal of pharmaceutical and biomedical analysis 51.3(2010):606-616. |
入库方式: OAI收割
来源:大连化学物理研究所
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