Carbohydrate separation by hydrophilic interaction liquid chromatography on a 'click' maltose column
文献类型：期刊论文
| 作者 | Fu, Qing1; Liang, Tu2; Zhang, Xiuli1; Du, Yuguang1; Guo, Zhimou1; Liang, Xinmiao1,2 |
| 刊名 | carbohydrate research
 |
| 出版日期 | 2010-12-10 |
| 卷号 | 345期号:18页码:2690-2697 |
| 关键词 | Oligosaccharides HILIC Click maltose Separation Purification |
| 英文摘要 | a general and efficient hydrophobic interaction liquid chromatography (hilic) method has been developed for the separation of various kinds of carbohydrates ranging from galactooligosaccharides carrageenan oligosaccharides sodium alginate chitooligosaccharides to higher molecular weight fructooligosaccharides three types of oligosaccharides (acidic basic and neutral) were purified by semi-preparative hilic as a result 18 oligosaccharides in high purity were obtained and their degrees of polymerization ranged from dp 2 to 7 furthermore oligosaccharides of plant origin were enriched and fractionated by solid-phase extraction (spe) on a graphitized carbon cartridge the oligosaccharide fractions that eluted from the cartridge were purified and then characterized by esims and nmr spectroscopy this strategy has led to the separation of a homogeneous raffinose family of oligosaccharides since the present method is universal efficient and stable separation and purification of various types of carbohydrates by hilic seem to be possible (c) 2010 elsevier ltd all rights reserved |
| WOS标题词 | science & technology ; life sciences & biomedicine ; physical sciences |
| 类目[WOS] | biochemistry & molecular biology ; chemistry, applied ; chemistry, organic |
| 研究领域[WOS] | biochemistry & molecular biology ; chemistry |
| 关键词[WOS] | anion-exchange chromatography ; ionization mass-spectrometry ; solid-phase extraction ; graphitized carbon ; polar compounds ; oligosaccharides ; monosaccharides ; glycopeptides ; hplc ; derivatization |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000285657700016 |
| 公开日期 | 2015-11-17 |
| 源URL | [http://159.226.238.44/handle/321008/142247]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | 1.Chinese Acad Sci, Dalian Inst Chem Phys, Key Lab Separat Sci Analyt Chem, Dalian 116023, Peoples R China 2.E China Univ Sci & Technol, Engn Res Ctr Pharmaceut Proc Chem, Minist Educ, Sch Pharm, Shanghai 200237, Peoples R China |
| 推荐引用方式 GB/T 7714 | Fu, Qing,Liang, Tu,Zhang, Xiuli,et al. Carbohydrate separation by hydrophilic interaction liquid chromatography on a 'click' maltose column[J]. carbohydrate research,2010,345(18):2690-2697. |
| APA | Fu, Qing,Liang, Tu,Zhang, Xiuli,Du, Yuguang,Guo, Zhimou,&Liang, Xinmiao.(2010).Carbohydrate separation by hydrophilic interaction liquid chromatography on a 'click' maltose column.carbohydrate research,345(18),2690-2697. |
| MLA | Fu, Qing,et al."Carbohydrate separation by hydrophilic interaction liquid chromatography on a 'click' maltose column".carbohydrate research 345.18(2010):2690-2697. |
入库方式： OAI收割
来源：大连化学物理研究所
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