A Headspace Cooled-liquid Phase Microextraction Technique and Its Application for Analysis of Fusel Oil in Water Samples and Volatile Compounds in Beer
文献类型：期刊论文
| 作者 | Chen Shi-Heng1,2; Wang Jian-Wei1; Li Wei-Wei1; Peng Hong1; Guan Ya-Feng1 |
| 刊名 | chinese journal of analytical chemistry
 |
| 出版日期 | 2011-05-01 |
| 卷号 | 39期号:5页码:675-679 |
| 关键词 | Headspace cooled-liquid phase microextraction Thermoelectric cooler Gas chromatography Fusel oil Beer |
| 英文摘要 | a novel headspace cooled-liquid phase microextraction (hs-clpme) has been developed and demonstrated. a polytetrafluoroethylene vial cap with a two-step cylindrical cavity was used as solvent drop holder, and a cooling system based on thermoelectric cooler (tec) was used to lower the temperature of solvent drop to subzero. volatile solvents can be used as extractant in hs-clpme, which extends the selection of extractant for hs-lpme, reduces the interference of the large solvent peak to the analytes peaks, and enhances the compatibility of hs-lpme with gas chromatograph (gc). because of the relatively lower temperature of extractant, the extraction efficiency has been improved. hs-clpme was applied to analyze the fusel oil in water. the operation parameters including the ionic intensity, the volume and temperature of extractant, the sample temperature, stirring rate, and extraction time were optimized. the limits of detections ranged from 0. 09 mu g/l to 0. 26 mu g/l for fusel oil, and the enrichment factors were from 78 to 198. the hs-clpme was also applied to analyze volatile flavors in beer. |
| WOS标题词 | science & technology ; physical sciences |
| 类目[WOS] | chemistry, analytical |
| 研究领域[WOS] | chemistry |
| 关键词[WOS] | single-drop microextraction ; solvent microextraction ; chlorobenzenes |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000293202300013 |
| 公开日期 | 2015-11-17 |
| 源URL | [http://159.226.238.44/handle/321008/142517]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | 1.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatog R&A Ctr, Dept Instrumentat & Analyt Chem,Key Lab Separat S, Dalian 116023, Peoples R China 2.Chinese Acad Sci, Grad Sch, Beijing 100039, Peoples R China |
| 推荐引用方式 GB/T 7714 | Chen Shi-Heng,Wang Jian-Wei,Li Wei-Wei,et al. A Headspace Cooled-liquid Phase Microextraction Technique and Its Application for Analysis of Fusel Oil in Water Samples and Volatile Compounds in Beer[J]. chinese journal of analytical chemistry,2011,39(5):675-679. |
| APA | Chen Shi-Heng,Wang Jian-Wei,Li Wei-Wei,Peng Hong,&Guan Ya-Feng.(2011).A Headspace Cooled-liquid Phase Microextraction Technique and Its Application for Analysis of Fusel Oil in Water Samples and Volatile Compounds in Beer.chinese journal of analytical chemistry,39(5),675-679. |
| MLA | Chen Shi-Heng,et al."A Headspace Cooled-liquid Phase Microextraction Technique and Its Application for Analysis of Fusel Oil in Water Samples and Volatile Compounds in Beer".chinese journal of analytical chemistry 39.5(2011):675-679. |
入库方式： OAI收割
来源：大连化学物理研究所
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