Isolation and quantitative determination of inulin-type oligosaccharides in roots of Morinda officinalis
文献类型：期刊论文
| 作者 | Yang, Zhenmin1,2; Hu, Jun1; Zhao, Mingyue1 |
| 刊名 | carbohydrate polymers
 |
| 出版日期 | 2011-02-01 |
| 卷号 | 83期号:4页码:1997-2004 |
| 关键词 | Inulin-type oligosaccharides Isolation Quantitative determination HPLC-ELSD Cyclodextrin-bond column |
| 英文摘要 | inulin-type oligosaccharides with different degree of polymerization (dp) were isolated from the traditional chinese medicine: morina officinalis by size-exclusion chromatography, and their purities were determined by hplc-elsd equipped with cyclodextrin-bond column. through analysis, the purities of obtained inulin-type oligosaccharides were higher more than 98% by one-step process. the structures of inulin-type oligosaccharides were confirmed by a combination of nmr, ms as well as comparison with already existing nmr data. using d-fructose and the isolated inulin-type oligosaccharides as standards, a determination method of monosaccharide and inulin-type oligosaccharides in morinda officinalis was first developed and validated. the validated method was successfully applied to analyze monosaccharide and oligosaccharides in three types of roots of m. officinalis and provided a new basis of assessment on quality of m. officinalis. (c) 2010 elsevier ltd. all rights reserved. |
| WOS标题词 | science & technology ; physical sciences |
| 类目[WOS] | chemistry, applied ; chemistry, organic ; polymer science |
| 研究领域[WOS] | chemistry ; polymer science |
| 关键词[WOS] | cyclodextrin-bonded phase ; structural-characterization ; pc12 cells ; medicine ; nmr ; fructooligosaccharides ; polysaccharides ; corticosterone ; identification ; trisaccharides |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000286965400075 |
| 公开日期 | 2015-11-17 |
| 源URL | [http://159.226.238.44/handle/321008/142528]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | 1.Zhengzhou Tobacco Res Inst CNTC, Lab Flavor & Fragrance, Zhengzhou 450001, Peoples R China 2.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatog R&A Ctr, Dalian 116023, Peoples R China |
| 推荐引用方式 GB/T 7714 | Yang, Zhenmin,Hu, Jun,Zhao, Mingyue. Isolation and quantitative determination of inulin-type oligosaccharides in roots of Morinda officinalis[J]. carbohydrate polymers,2011,83(4):1997-2004. |
| APA | Yang, Zhenmin,Hu, Jun,&Zhao, Mingyue.(2011).Isolation and quantitative determination of inulin-type oligosaccharides in roots of Morinda officinalis.carbohydrate polymers,83(4),1997-2004. |
| MLA | Yang, Zhenmin,et al."Isolation and quantitative determination of inulin-type oligosaccharides in roots of Morinda officinalis".carbohydrate polymers 83.4(2011):1997-2004. |
入库方式： OAI收割
来源：大连化学物理研究所
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