中国科学院机构知识库网格
Chinese Academy of Sciences Institutional Repositories Grid
The properties of silica nanoparticles with high monodispersity synthesized in the microreactor system

文献类型:期刊论文

作者Su, Min1,2; Su, Hongjiu1; Du, Baolei1,2; Li, Xiaotong1,2; Ren, Gaoyuan1; Wang, Shudong1
刊名journal of sol-gel science and technology
出版日期2014-11-01
卷号72期号:2页码:375-384
关键词Microreactor Particle size Silica Nanoparticle Silica nanoparticle
英文摘要a new combined micromixer/microreactor/batch reactor system for the synthesis of monodisperse silica particles was demonstrated, which showed superiorities over the batch reactor. the silica nanoparticles with different sizes (ranging from 20 nm to 2 mu m) and size distributions could be controllably synthesized by varying the reaction temperature and reaction time. the narrowest size distribution of the silica particles was synthesized at 60 degrees c. the transmission electron microscopy characterization showed that the sphericities of silica particles got better as the particle size increased. thermal gravimetry-differential thermal analysis and fourier transform infrared characterization indicated that the amount of ethoxy groups of silica particles decreased and the hydroxyl groups increased with the reaction time increasing. and the hydroxyl groups in silica particles increased with the reaction temperature rising.
WOS标题词science & technology ; technology
类目[WOS]materials science, ceramics
研究领域[WOS]materials science
关键词[WOS]tunable pore-size ; sol-gel ; mesoporous carbon ; growth-process ; particles ; polymerization ; hydrolysis ; catalyst ; porosity ; support
收录类别SCI
语种英语
WOS记录号WOS:000343131000021
公开日期2015-11-17
源URL[http://159.226.238.44/handle/321008/143184]  
专题大连化学物理研究所_中国科学院大连化学物理研究所
作者单位1.Chinese Acad Sci, Dalian Inst Chem Phys, Dalian Natl Lab Clean Energy, Dalian 116023, Peoples R China
2.Univ Chinese Acad Sci, Beijing 100049, Peoples R China
推荐引用方式
GB/T 7714
Su, Min,Su, Hongjiu,Du, Baolei,et al. The properties of silica nanoparticles with high monodispersity synthesized in the microreactor system[J]. journal of sol-gel science and technology,2014,72(2):375-384.
APA Su, Min,Su, Hongjiu,Du, Baolei,Li, Xiaotong,Ren, Gaoyuan,&Wang, Shudong.(2014).The properties of silica nanoparticles with high monodispersity synthesized in the microreactor system.journal of sol-gel science and technology,72(2),375-384.
MLA Su, Min,et al."The properties of silica nanoparticles with high monodispersity synthesized in the microreactor system".journal of sol-gel science and technology 72.2(2014):375-384.

入库方式: OAI收割

来源:大连化学物理研究所

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