Solvothermal synthesis and characterization of silica-pillared titanium phosphate
文献类型：期刊论文
| 作者 | Jiao, XL; Chen, DR; Pang, WQ; Xu, RR; Yue, Y |
| 刊名 | JOURNAL OF MATERIALS CHEMISTRY
 |
| 出版日期 | 1998-12-01 |
| 卷号 | 8期号:12页码:2831-2834 |
| 英文摘要 | Silica-pillared titanium phosphate has been synthesized from Ti(OC4H9)(4)-H3PO4-H2N(CH2)(3)Si (OC2H5)(3)-C2H5OH and characterized by XRD, SEM, IR and TGA. The synthesis conditions were investigated and the optimal conditions are reported: crystallization at 180 degrees C for about 7 days with a batch composition of 1.0 Ti(OC4H9)(4):3.6 H3PO4: 1.0 H2N(CH2)(3)Si(OC2H5)(3):33 C2H5OH. XRD analysis gives the lattice parameters of the monoclinic cell as a = 1.99952 nm, b = 0.41803 nm, c = 0.90062 mm, beta = 97.462 degrees, V = 0.74642 nm(3), and Z = 2. N-2 adsorption-desorption test shows that the pillared compound has a BET surface area of 51 m(2) g(-1) |
| WOS标题词 | Science & Technology ; Physical Sciences ; Technology |
| 类目[WOS] | Chemistry, Physical ; Materials Science, Multidisciplinary |
| 研究领域[WOS] | Chemistry ; Materials Science |
| 关键词[WOS] | ALPHA-ZIRCONIUM PHOSPHATE ; NUCLEAR MAGNETIC-RESONANCE ; C-13 CROSS-POLARIZATION ; OCTAMERIC SILOXANES ; INTERCALATION ; SI-29 |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000077690800044 |
| 公开日期 | 2015-12-01 |
| 源URL | [http://ir.wipm.ac.cn/handle/112942/8279]  |
| 专题 | 武汉物理与数学研究所_2011年以前论文发表（包括2011年） |
| 作者单位 | 1.Jilin Univ, Dept Chem, Changchun 130023, Peoples R China 2.Shandong Univ, Dept Chem, Jinan 250100, Peoples R China 3.Chinese Acad Sci, Wuhan Inst Phys, Wuhan 430071, Peoples R China |
| 推荐引用方式 GB/T 7714 | Jiao, XL,Chen, DR,Pang, WQ,et al. Solvothermal synthesis and characterization of silica-pillared titanium phosphate[J]. JOURNAL OF MATERIALS CHEMISTRY,1998,8(12):2831-2834. |
| APA | Jiao, XL,Chen, DR,Pang, WQ,Xu, RR,&Yue, Y.(1998).Solvothermal synthesis and characterization of silica-pillared titanium phosphate.JOURNAL OF MATERIALS CHEMISTRY,8(12),2831-2834. |
| MLA | Jiao, XL,et al."Solvothermal synthesis and characterization of silica-pillared titanium phosphate".JOURNAL OF MATERIALS CHEMISTRY 8.12(1998):2831-2834. |
入库方式： OAI收割
来源：武汉物理与数学研究所
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