Synthesis of La(III), Y(III) complexes with polyglycol aldehyde-amino acid Schiff base and their high resolution solid state C-13 NMR spectra
文献类型：期刊论文
| 作者 | Li, N; Yao, KM; Lou, KY; Shen, LF; Yuan, HZ |
| 刊名 | SCIENCE IN CHINA SERIES B-CHEMISTRY
 |
| 出版日期 | 1999-12-01 |
| 卷号 | 42期号:6页码:599-604 |
| 关键词 | Ln(III) complexes with Schiff base high resolution solid state C-13 NMR liquid state 2D-H-1-C-13 COSYNMR CPMAS TOSS |
| 英文摘要 | La(III),Y(III) complexes with diglycol aldehyde bis-arginine (H(2)DAAR) and tetraglycol aldehyde bis-lysine (H(2)TALY) Schiff bases were synthesized. They were characterized and formulated as La( H(2)DAAR)(NO3)(3). 6H(2)O and Y(H(2)TALY) (NO3)(3) . 5H(2)O separately by elemental analyses. The obtained complexes were investigated in detail by high resolution solid state (HRSS) C-13 NMR using cross polarization, magic angle spinning (CPMAS), and total suppression of sidebands (TOSS) techniques. The results are supported by the liquid state 2D-(1) H-C-13 COSY NMR spectra. Some new information about the splitting peaks of C-13 for -CH=N- soup and alkene carbon bands, etc. in HRSS C-13 NMR spectra are given. |
| WOS标题词 | Science & Technology ; Physical Sciences |
| 类目[WOS] | Chemistry, Multidisciplinary |
| 研究领域[WOS] | Chemistry |
| 关键词[WOS] | GADOLINIUM COMPLEXES ; EPR-SPECTRA |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000084653800006 |
| 公开日期 | 2015-12-01 |
| 源URL | [http://ir.wipm.ac.cn/handle/112942/8362]  |
| 专题 | 武汉物理与数学研究所_2011年以前论文发表（包括2011年） |
| 作者单位 | 1.Zhejiang Univ, Dept Chem, Hangzhou 310027, Peoples R China 2.Chinese Acad Sci, Wuhan Inst Phys & Math, State Key Lab Magnet Resonance & Atom & Mol Phys, Wuhan 430071, Peoples R China |
| 推荐引用方式 GB/T 7714 | Li, N,Yao, KM,Lou, KY,et al. Synthesis of La(III), Y(III) complexes with polyglycol aldehyde-amino acid Schiff base and their high resolution solid state C-13 NMR spectra[J]. SCIENCE IN CHINA SERIES B-CHEMISTRY,1999,42(6):599-604. |
| APA | Li, N,Yao, KM,Lou, KY,Shen, LF,&Yuan, HZ.(1999).Synthesis of La(III), Y(III) complexes with polyglycol aldehyde-amino acid Schiff base and their high resolution solid state C-13 NMR spectra.SCIENCE IN CHINA SERIES B-CHEMISTRY,42(6),599-604. |
| MLA | Li, N,et al."Synthesis of La(III), Y(III) complexes with polyglycol aldehyde-amino acid Schiff base and their high resolution solid state C-13 NMR spectra".SCIENCE IN CHINA SERIES B-CHEMISTRY 42.6(1999):599-604. |
入库方式： OAI收割
来源：武汉物理与数学研究所
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