中国科学院机构知识库网格
Chinese Academy of Sciences Institutional Repositories Grid
Synthesis of large single crystals of silica-sodalite and silicalite-1 in the presence of pyrocatechol

文献类型:期刊论文

作者Shao, CL; Li, XT; Qiu, SL; Xiao, FS; Zhang, ZT; Wei, B; Wang, RW; Yue, Y
刊名CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE
出版日期1999-11-01
卷号20期号:11页码:1667-1670
关键词silica-sodalite silicalite-1 large single crystals pyrocatechol silicon-pyrocatechol complex
英文摘要To obtain large perfect crystals of zeolites, pyrocatechol as an additive was added into the two system: SiO2-NaOH-EG-R and SiO2-TPABr-NaOH-R-H2O (R: pyrocatechol, EG: ethylene glycol), Experimental results showed that the crystals synthesized in the presence of pyrocatechol have much larger size and better morphology than those synthesized in the absence of pyrocatechol, The role of pyrocatechol in the hydrothermal reaction mixture has been characterized by Si-29 NMR, IR, and UV-Vis spectroscopy, and it was shown that silicon-pyrocatechol complex was formed in the reaction system.
WOS标题词Science & Technology ; Physical Sciences
类目[WOS]Chemistry, Multidisciplinary
研究领域[WOS]Chemistry
关键词[WOS]GROWTH ; CRYSTALLIZATION ; SYSTEM ; ZSM-5
收录类别SCI
语种英语
WOS记录号WOS:000083723600002
公开日期2015-12-01
源URL[http://ir.wipm.ac.cn/handle/112942/8441]  
专题武汉物理与数学研究所_2011年以前论文发表(包括2011年)
作者单位1.Jilin Univ, Dept Chem, Changchun 130023, Peoples R China
2.Jilin Univ, Key Lab Inorgan Synth & Preparat Chem, Changchun 130023, Peoples R China
3.Chinese Acad Sci, Wuhan Inst Phys, Wuhan 430000, Peoples R China
推荐引用方式
GB/T 7714
Shao, CL,Li, XT,Qiu, SL,et al. Synthesis of large single crystals of silica-sodalite and silicalite-1 in the presence of pyrocatechol[J]. CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE,1999,20(11):1667-1670.
APA Shao, CL.,Li, XT.,Qiu, SL.,Xiao, FS.,Zhang, ZT.,...&Yue, Y.(1999).Synthesis of large single crystals of silica-sodalite and silicalite-1 in the presence of pyrocatechol.CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE,20(11),1667-1670.
MLA Shao, CL,et al."Synthesis of large single crystals of silica-sodalite and silicalite-1 in the presence of pyrocatechol".CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE 20.11(1999):1667-1670.

入库方式: OAI收割

来源:武汉物理与数学研究所

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