Recovery of underwater resonances by magnetization transferred NMR spectroscopy (RECUR-NMR)
文献类型：期刊论文
| 作者 | Liu, ML; Tang, HR; Nicholson, JK; Lindon, JC |
| 刊名 | JOURNAL OF MAGNETIC RESONANCE
 |
| 出版日期 | 2001-11-01 |
| 卷号 | 153期号:1页码:133-137 |
| 英文摘要 | A method for detecting small molecule NMR resonances under a water peak in biological samples is presented. After high-efficiency solvent suppression using double WATERGATE, either a TOCSY- or ROESY-based coherence transfer sequence is applied to reestablish the resonances close to, or under, water through magnetization transfer using scalar or dipolar coupling, respectively. The use of the TOCSY and ROESY methods ensures an in-phase magnetization transfer, which makes the new approach readily extended for the measurement of transverse relaxation times, internuclear ROEs, and ROE buildup rates. An extension of the new approach for J-resolved spectroscopy is also presented and tested using a sample of human blood plasma. (C) 2001 Academic Press. |
| WOS标题词 | Science & Technology ; Life Sciences & Biomedicine ; Physical Sciences ; Technology |
| 类目[WOS] | Biochemical Research Methods ; Physics, Atomic, Molecular & Chemical ; Spectroscopy |
| 研究领域[WOS] | Biochemistry & Molecular Biology ; Physics ; Spectroscopy |
| 关键词[WOS] | WATER-SUPPRESSION ; SOLVENT SUPPRESSION ; SELECTIVE DETECTION ; H-1-NMR RESONANCES ; PULSE SEQUENCES ; SENSITIVITY |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000172245000016 |
| 公开日期 | 2015-12-08 |
| 源URL | [http://ir.wipm.ac.cn/handle/112942/8619]  |
| 专题 | 武汉物理与数学研究所_2011年以前论文发表（包括2011年） |
| 作者单位 | 1.Univ London Imperial Coll Sci Technol & Med, Fac Med, London SW7 2AZ, England 2.Chinese Acad Sci, Wuhan Inst Phys & Math, Lab Magnet Resonance & Atom, Wuhan 430071, Peoples R China 3.Chinese Acad Sci, Wuhan Inst Phys & Math, Mol Phys Lab, Wuhan 430071, Peoples R China |
| 推荐引用方式 GB/T 7714 | Liu, ML,Tang, HR,Nicholson, JK,et al. Recovery of underwater resonances by magnetization transferred NMR spectroscopy (RECUR-NMR)[J]. JOURNAL OF MAGNETIC RESONANCE,2001,153(1):133-137. |
| APA | Liu, ML,Tang, HR,Nicholson, JK,&Lindon, JC.(2001).Recovery of underwater resonances by magnetization transferred NMR spectroscopy (RECUR-NMR).JOURNAL OF MAGNETIC RESONANCE,153(1),133-137. |
| MLA | Liu, ML,et al."Recovery of underwater resonances by magnetization transferred NMR spectroscopy (RECUR-NMR)".JOURNAL OF MAGNETIC RESONANCE 153.1(2001):133-137. |
入库方式： OAI收割
来源：武汉物理与数学研究所
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