Separation of biogenic amines by micellar electrokinetic chromatography
文献类型:期刊论文
作者 | Qiao Cheng-Dong; Song Ping-Shun; Yan Xiang; Jiang Sheng-Xiang |
刊名 | Chinese journal of analytical chemistry
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出版日期 | 2007 |
卷号 | 35期号:1页码:95-98 |
关键词 | Micellar electrokinetic chromatography Separation Biogenic amines 5-methoxy tryptamine D L-5-hydroxytryptophan |
ISSN号 | 0253-3820 |
通讯作者 | Jiang sheng-xiang(sxjiang@lab.ac.cn) |
英文摘要 | A novel, simple and rapid method for the separation of biogenic amines by micellar electrokinetic chromatography with diode array detection was developed. the effect of some key factors, such as concentration of buffer and sodium dodecyl sulfate (sds), ph, surfactant, capillary temperature and applied voltage on the separation of biogenic amines was investigated. under the optimized conditions, the baseline separation of five blogenic amines was achieved with satisfactory repeatability and high separation efficiency in 7 min using 40 mmol/l borate buffer (ph 8. 5) containing 68 mmol/l sds, under 25 kv applied voltage at 25 degrees c. the linear range, the limit of detection and the repeatability were also investigated under the optimized conditions. the rsd (n = 6) of the migration time is < 0. 8% and the rsd (n = 6) of peak area is less than 4% for each blogenic amines, the linear ranges are wide and the limit of detection is low. |
WOS关键词 | RED WINES ; FOODS |
WOS研究方向 | Chemistry |
WOS类目 | Chemistry, Analytical |
语种 | 英语 |
WOS记录号 | WOS:000246604700019 |
出版者 | SCIENCE CHINA PRESS |
URI标识 | http://www.irgrid.ac.cn/handle/1471x/2380033 |
专题 | 中国科学院大学 |
通讯作者 | Jiang Sheng-Xiang |
作者单位 | 1.Chinese Acad Sci, Lanzhou Inst Chem Phys, Key Lab Nat Med Gansu Prov, Lanzhou 730000, Peoples R China 2.Lanzhou Univ, Hosp 1, Lanzhou 730000, Peoples R China 3.Gansu Prov Inst Drug Control, Lanzhou 730000, Peoples R China 4.Chinese Acad Sci, Grad Sch, Beijing 10039, Peoples R China |
推荐引用方式 GB/T 7714 | Qiao Cheng-Dong,Song Ping-Shun,Yan Xiang,et al. Separation of biogenic amines by micellar electrokinetic chromatography[J]. Chinese journal of analytical chemistry,2007,35(1):95-98. |
APA | Qiao Cheng-Dong,Song Ping-Shun,Yan Xiang,&Jiang Sheng-Xiang.(2007).Separation of biogenic amines by micellar electrokinetic chromatography.Chinese journal of analytical chemistry,35(1),95-98. |
MLA | Qiao Cheng-Dong,et al."Separation of biogenic amines by micellar electrokinetic chromatography".Chinese journal of analytical chemistry 35.1(2007):95-98. |
入库方式: iSwitch采集
来源:中国科学院大学
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