Study on synthesis of 2-amino-2 '-hydroxy-1,1 '-binaphthyl by two-phase oxidative coupling with a cyclic solid oxidant
文献类型：期刊论文
| 作者 | Jiang Yi; Wang Juan-Yun; Chen Jun-He; Wang Wei-Jun; Yan Han; Zhang Xiao-Xia; Wang Chao; Zhang Guo-Lin; Li Bo-Gang |
| 刊名 | Acta chimica sinica
 |
| 出版日期 | 2007-09-14 |
| 卷号 | 65期号:17页码:1925-1928 |
| 关键词 | 2-naphthol 2-naphthylarmine Solid-oxidant Cross-coupling 2-amino-2 '-hydroxy-1,1 '-binaphthyl |
| ISSN号 | 0567-7351 |
| 通讯作者 | Jiang yi(yjiang@cioc.ac.cn) |
| 英文摘要 | Various solid-oxidants with different loadings of fecl3 on al2o3 were prepared by impregnation. the effects of support and solvent on the oxidative cross-coupling of 2-naphthol with 2-naphthylamine using fecl3/al2o3 were studied. up to 95.01% yield of 2-amino-2'-hydroxy-1,1'-binaphthyl (nobin) was obtained in chlorobenzene using the oxidant with 10% fecl3 loading on the support containing 5% tio2 at 60 degrees c. the activity of the used oxidant was improved by treatment with h2o2, which provided an effective method to regenerate the solid-oxidant. |
| WOS研究方向 | Chemistry |
| WOS类目 | Chemistry, Multidisciplinary |
| 语种 | 英语 |
| WOS记录号 | WOS:000249894200034 |
| 出版者 | SCIENCE CHINA PRESS |
| URI标识 | http://www.irgrid.ac.cn/handle/1471x/2381353 |
| 专题 | 中国科学院大学 |
| 通讯作者 | Jiang Yi |
| 作者单位 | 1.Chinese Acad Sci, Chengdu Inst Organ Chem, Chengdu 610041, Peoples R China 2.Chinese Acad Sci, Chengdu Inst Biol, Chengdu 610041, Peoples R China 3.Chinese Acad Sci, Grad Sch, Beijing 100039, Peoples R China |
| 推荐引用方式 GB/T 7714 | Jiang Yi,Wang Juan-Yun,Chen Jun-He,et al. Study on synthesis of 2-amino-2 '-hydroxy-1,1 '-binaphthyl by two-phase oxidative coupling with a cyclic solid oxidant[J]. Acta chimica sinica,2007,65(17):1925-1928. |
| APA | Jiang Yi.,Wang Juan-Yun.,Chen Jun-He.,Wang Wei-Jun.,Yan Han.,...&Li Bo-Gang.(2007).Study on synthesis of 2-amino-2 '-hydroxy-1,1 '-binaphthyl by two-phase oxidative coupling with a cyclic solid oxidant.Acta chimica sinica,65(17),1925-1928. |
| MLA | Jiang Yi,et al."Study on synthesis of 2-amino-2 '-hydroxy-1,1 '-binaphthyl by two-phase oxidative coupling with a cyclic solid oxidant".Acta chimica sinica 65.17(2007):1925-1928. |
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来源：中国科学院大学
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