Quantitative analysis of genistein in human plasma by online concentration ce with uv detection
文献类型:期刊论文
作者 | Feng, Hai-Yan1,2; Hou, Shu-Rong1; Zheng, Na1; Li, Xiang-Jun1; Hu, Zhong-Bo1; Yuan, Zhuo-Bin1 |
刊名 | Chromatographia
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出版日期 | 2008-09-01 |
卷号 | 68期号:5-6页码:431-435 |
关键词 | Capillary electrophoresis Online acid barrage stacking Genistein Plasma |
ISSN号 | 0009-5893 |
DOI | 10.1365/s10337-008-0658-7 |
通讯作者 | Li, xiang-jun(lixiangj@gucas.ac.cn) |
英文摘要 | A rapid capillary electrophoresis method based on online acid barrage stacking has been successfully established for analysis of trace amounts of genistein in human plasma. genistein was analyzed within 8 min, with 200 mmol l(-1) citric acid (ph 1.7) as acid barrage, and injection times of 180 and 30 s for sample and acid, respectively. good linearity was obtained in the range 0.05-5 mg l(-1) and the limit of detection was 0.03 mg l(-1). compared with normal sample injection, this method resulted in more than a fiftyfold improvement in detection sensitivity. the technique has potential for use in studies of genistein metabolism and of exposure levels in humans. |
WOS关键词 | PERFORMANCE LIQUID-CHROMATOGRAPHY ; CAPILLARY-ELECTROPHORESIS ; ELECTROCHEMICAL DETECTION ; ISOFLAVONE AGLYCONES ; MASS-SPECTROMETRY ; DAIDZEIN |
WOS研究方向 | Biochemistry & Molecular Biology ; Chemistry |
WOS类目 | Biochemical Research Methods ; Chemistry, Analytical |
语种 | 英语 |
WOS记录号 | WOS:000259186700019 |
出版者 | SPRINGER HEIDELBERG |
URI标识 | http://www.irgrid.ac.cn/handle/1471x/2390973 |
专题 | 中国科学院大学 |
通讯作者 | Li, Xiang-Jun |
作者单位 | 1.Chinese Acad Sci, Grad Univ, Coll Chem & Chem Engn, Beijing 100049, Peoples R China 2.Shijiazhuang Univ, Sch Chem Engn, Shijiazhuang 050035, Peoples R China |
推荐引用方式 GB/T 7714 | Feng, Hai-Yan,Hou, Shu-Rong,Zheng, Na,et al. Quantitative analysis of genistein in human plasma by online concentration ce with uv detection[J]. Chromatographia,2008,68(5-6):431-435. |
APA | Feng, Hai-Yan,Hou, Shu-Rong,Zheng, Na,Li, Xiang-Jun,Hu, Zhong-Bo,&Yuan, Zhuo-Bin.(2008).Quantitative analysis of genistein in human plasma by online concentration ce with uv detection.Chromatographia,68(5-6),431-435. |
MLA | Feng, Hai-Yan,et al."Quantitative analysis of genistein in human plasma by online concentration ce with uv detection".Chromatographia 68.5-6(2008):431-435. |
入库方式: iSwitch采集
来源:中国科学院大学
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