Preparation of novel chiral stationary phase based on click chemistry for ligand exchange chromatography
文献类型：期刊论文
| 作者 | Fu, Chun Mei1; Shi, Hong Yu2,3; Qian, Guang Sheng1; Li, Zhang Wan1 |
| 刊名 | Chinese chemical letters
 |
| 出版日期 | 2009-11-01 |
| 卷号 | 20期号:11页码:1345-1347 |
| 关键词 | Click chemistry Ligand exchange chromatography Chiral stationary phase Dl-amino acids |
| ISSN号 | 1001-8417 |
| DOI | 10.1016/j.cclet.2009.05.011 |
| 通讯作者 | Li, zhang wan(lizhangwanlab@163.com) |
| 英文摘要 | Click chemistry was applied to immobilize l-proline derivative onto azide-modified silica gel to give a novel chiral stationary phase (denoted as click-csp) for ligand exchange chromatography. the developed protocol combines the benefits of operational simplicity, exceptionally mild conditions and high surface loadings. the enantioselectivity alpha of some dl-amino acids on the click-csp were found to be in the range from 1.13 to 3.46. the chromatographic resolutions of some dl-amino acids and the stability study firmly illustrate the potential of click chemistry for preparation chiral stationary phase for ligand exchange chromatography. (c) 2009 zhang wan li. published by elsevier b.v. on behalf of chinese chemical society. all rights reserved. |
| WOS关键词 | LIQUID-CHROMATOGRAPHY ; SEPARATION |
| WOS研究方向 | Chemistry |
| WOS类目 | Chemistry, Multidisciplinary |
| 语种 | 英语 |
| WOS记录号 | WOS:000272150800022 |
| 出版者 | ELSEVIER SCIENCE INC |
| URI标识 | http://www.irgrid.ac.cn/handle/1471x/2403622 |
| 专题 | 中国科学院大学 |
| 通讯作者 | Li, Zhang Wan |
| 作者单位 | 1.Sichuan Univ, W China Sch Pharm, Chengdu 610041, Peoples R China 2.Chinese Acad Sci, Chengdu Inst Organ Chem, Chengdu 610041, Peoples R China 3.Chinese Acad Sci, Grad Sch, Beijing 100049, Peoples R China |
| 推荐引用方式 GB/T 7714 | Fu, Chun Mei,Shi, Hong Yu,Qian, Guang Sheng,et al. Preparation of novel chiral stationary phase based on click chemistry for ligand exchange chromatography[J]. Chinese chemical letters,2009,20(11):1345-1347. |
| APA | Fu, Chun Mei,Shi, Hong Yu,Qian, Guang Sheng,&Li, Zhang Wan.(2009).Preparation of novel chiral stationary phase based on click chemistry for ligand exchange chromatography.Chinese chemical letters,20(11),1345-1347. |
| MLA | Fu, Chun Mei,et al."Preparation of novel chiral stationary phase based on click chemistry for ligand exchange chromatography".Chinese chemical letters 20.11(2009):1345-1347. |
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来源：中国科学院大学
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