Applications of titania and zirconia hollow fibers in sorptive microextraction of n,n-dimethylacetamide from water sample
文献类型：期刊论文
| 作者 | Li, Jia1,2; Qi, Huan-Yang1; Shi, Yan-Ping1 |
| 刊名 | Analytica chimica acta
 |
| 出版日期 | 2009-10-05 |
| 卷号 | 651期号:2页码:182-187 |
| 关键词 | Titania hollow fiber Zirconia hollow fiber Hollow fiber sorptive extraction N,n-dimethylacetamide Gas chromatography |
| ISSN号 | 0003-2670 |
| DOI | 10.1016/j.aca.2009.08.031 |
| 通讯作者 | Shi, yan-ping(shiyp@lzb.ac.cn) |
| 英文摘要 | The convenient fabrications of titania and zirconia hollow fiber with three-dimensional porous structure using polypropylene hollow fibers as templates were developed. and an analytical method based on enrichment and extraction of analytes in the water sample, hollow fiber sorptive microextraction in combined with gas chromatography has been developed for the rapid analysis of n,n-dimethylacetamide (dma) in the environmental samples. the results showed that zirconia hollow fiber gave higher extraction performance of dma than that of titania hollow fiber. the method validations, including linearity, limit of detection, limit of qualification, precision, and repeatability were investigated. linearity for six-point calibration curve was excellent with zirconia hollow fiber having r(2) value greater than 0.9993 at the linearity range of 0.001-10 mg ml(-1). in addition, it seems that hollow fiber sorptive extraction is a promising technique for the enrichment and purification of analytes extracted directly from liquid samples without any other pretreatment. (c) 2009 elsevier b.v. all rights reserved. |
| WOS关键词 | SOLID-PHASE MICROEXTRACTION ; LIQUID-CHROMATOGRAPHY ; AQUEOUS SAMPLES ; EXTRACTION ; GC |
| WOS研究方向 | Chemistry |
| WOS类目 | Chemistry, Analytical |
| 语种 | 英语 |
| WOS记录号 | WOS:000270745600007 |
| 出版者 | ELSEVIER SCIENCE BV |
| URI标识 | http://www.irgrid.ac.cn/handle/1471x/2405368 |
| 专题 | 中国科学院大学 |
| 通讯作者 | Shi, Yan-Ping |
| 作者单位 | 1.Chinese Acad Sci, Lanzhou Inst Chem Phys, Key Lab Nat Med Gansu Prov, Lanzhou 730000, Peoples R China 2.Chinese Acad Sci, Grad Univ, Beijing 100039, Peoples R China |
| 推荐引用方式 GB/T 7714 | Li, Jia,Qi, Huan-Yang,Shi, Yan-Ping. Applications of titania and zirconia hollow fibers in sorptive microextraction of n,n-dimethylacetamide from water sample[J]. Analytica chimica acta,2009,651(2):182-187. |
| APA | Li, Jia,Qi, Huan-Yang,&Shi, Yan-Ping.(2009).Applications of titania and zirconia hollow fibers in sorptive microextraction of n,n-dimethylacetamide from water sample.Analytica chimica acta,651(2),182-187. |
| MLA | Li, Jia,et al."Applications of titania and zirconia hollow fibers in sorptive microextraction of n,n-dimethylacetamide from water sample".Analytica chimica acta 651.2(2009):182-187. |
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来源：中国科学院大学
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