The melting and recrystallization behavior of poly(ethylene terephthalate)/SiO2 nanocomposites studied by Step-scan DSC
文献类型:会议论文
作者 | Liu, Chen; Zheng, Kang; Yao, Xia Yin; Zhang, Xian; Liu, Xiang Lan; Wang, Ruo Xi; Tian, Xing You |
出版日期 | 2010 |
会议日期 | AUG 19-21, 2009 |
关键词 | ISOTHERMAL CRYSTALLIZATION KINETICS POLY(ETHYLENE-TEREPHTHALATE) |
卷号 | 87-88 |
DOI | 10.4028/www.scientific.net/AMR.87-88.69 |
英文摘要 | The melting and recrystallization behavior of Poly(ethylene terephthalate) (PET)/SiO2 nanocomposites after isothermal crystallization from the melt was studied by Step-scan differential scanning calorimetry (SDSC). The influence of SiO2 contents, crystallization temperature and crystallization time on the melting process were examined. Two melting endotherms(in the SDSC C-P.A curves, reversible part) and one recrystallization exotherm (in the SDSC C-P.lsoK curves, irreversible part)of PET/SiO2 nanocomposites after isothermal crystallization were observed during the melt process. This ascribes to the melting-recrystallization mechanism. The low temperature endotherm attributes to the melting of primary crystal formed during the isothermal treating and the high temperature endotherm resulting from the melting of recrystallization materials. The reason why more recrystallization happened with the increase of SiO2 content was given and the process of recrystallization was described in detail. The effects of crystal perfection and recrystallization were minimized by increasing of crystallization temperature and time. |
会议录出版者 | Advanced Materials Research |
学科主题 | Polymer Science |
ISSN号 | 1022-6680 |
源URL | [http://ir.nimte.ac.cn/handle/174433/23723] ![]() |
专题 | 会议专题 会议专题_会议论文 |
推荐引用方式 GB/T 7714 | Liu, Chen,Zheng, Kang,Yao, Xia Yin,et al. The melting and recrystallization behavior of poly(ethylene terephthalate)/SiO2 nanocomposites studied by Step-scan DSC[C]. 见:. AUG 19-21, 2009. |
入库方式: OAI收割
来源:宁波材料技术与工程研究所
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