High-speed counter-current chromatography combined with column chromatography for isolation of methyllycaconitine from Delphinium pseudocyanthum
文献类型：期刊论文
| 作者 | Gu, DongYu; Yang, Yi; Zhong, Jie; Aisa, Haji Akber ; Zhang, TianYou
|
| 刊名 | CHROMATOGRAPHIA
 |
| 出版日期 | 2007 |
| 卷号 | 66期号:11-12页码:949-951 |
| ISSN号 | 0009-5893 |
| 关键词 | high-speed counter-current chromatography Delphinium pseudocyanthum methyllycaconitine |
| 通讯作者 | Aisa, HA |
| 中文摘要 | Preparative high-speed counter-current chromatography (HSCCC) combined with conventional column chromatography (CC) has been used for isolation and purification of methyllycaconitine from Delphinium pseudocyanthum. n-Hexane-ethyl acetate-methanol-water, 1:1:1:2 (v/v), was used as the solvent system for HSCCC. Separation of methyllycaconitine from an HSCCC fraction was successfully achieved by CC on silica gel using chloroform-methanol, 7:1 (v/v), as mobile phase. A total of 113.45 mg methyllycaconitine of purity > 95% was obtained from 1.044 g extract of D. pseudocyanthum. Its structure was identified by MS and NMR. |
| 收录类别 | SCI |
| WOS记录号 | WOS:000252089000021 |
| 公开日期 | 2014-11-11 |
| 源URL | [http://ir.xjipc.cas.cn/handle/365002/4114]  |
| 专题 | 新疆理化技术研究所_省部共建新疆特有药用资源利用重点实验室 |
| 作者单位 | Chinese Acad Sci, Xinjiang Key Lab Plant Resource & Natr Products C, Xinjiang Tech Inst Phys & Chem, Urumqi 830011, Peoples R China; Chinese Acad Sci, Grad Univ, Beijing 100049, Peoples R China;Beijing Inst New Technol Applicat, Beijing 100049, Peoples R China |
| 推荐引用方式 GB/T 7714 | Gu, DongYu,Yang, Yi,Zhong, Jie,et al. High-speed counter-current chromatography combined with column chromatography for isolation of methyllycaconitine from Delphinium pseudocyanthum[J]. CHROMATOGRAPHIA,2007,66(11-12):949-951. |
| APA | Gu, DongYu,Yang, Yi,Zhong, Jie,Aisa, Haji Akber,&Zhang, TianYou.(2007).High-speed counter-current chromatography combined with column chromatography for isolation of methyllycaconitine from Delphinium pseudocyanthum.CHROMATOGRAPHIA,66(11-12),949-951. |
| MLA | Gu, DongYu,et al."High-speed counter-current chromatography combined with column chromatography for isolation of methyllycaconitine from Delphinium pseudocyanthum".CHROMATOGRAPHIA 66.11-12(2007):949-951. |
入库方式： OAI收割
来源：新疆理化技术研究所
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