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	Reductive Benzylation of C-60 Imidazoline with a Bulky Addend 期刊论文 OAI收割 organic letters, 2014, 卷号: 16, 期号: 3, 页码: 712-715 Hou, Hui-Lei; Li, Zong-Jun; Gao, Xiang 收藏 \| 浏览/下载：31/0 \| 提交时间：2015/05/26 FULLERENES FUNCTIONALIZATION NUCLEOPHILES DERIVATIVES C-70(2-) ADDUCT NMR
	抗2型糖尿病药物“海普诺”的化学全合成方法专利 OAI收割专利类型: 发明, 专利号: CN200910017839.5, 申请日期: 2011-03-23, 公开日期: 2011-03-23 史大永; 郭书举; 李敬收藏 \| 浏览/下载：24/0 \| 提交时间：2014/08/04 一种抗2型糖尿病药物“海普诺”的化学全合成方法 (b)碘甲烷与化合物2摩尔比为1∶1～1∶1.5 (c)80％水合肼 (d)溴素与化合物3摩尔比为2∶1～3∶1 (e)硼氢化钠与化合物5摩尔比为1∶4～1∶3 (f)三氯化铝：化合物4：化合物6摩尔比为1∶1∶1 (g)N?溴代丁二酰亚胺与化合物7摩尔比为1.1∶1 (h)碳酸钾 (i)三溴化硼与化合物8摩尔比为6∶1～8∶1 (j)95％的乙醇其特征在于：所述的化合物合成路线为：(a)溴素与化合物1摩尔比为1∶1 碳酸钾氢氧化钾乙酸甲醇二氯甲烷催化剂 1 二氯甲烷 85％磷酸甲醇 N 二甘醇 60～70℃ 冰水浴室温四氯化碳 4?二氧六环与水体积比为1∶1 0℃ 70～80℃。F2009100178395C0000011.tif 冰水浴 N?二甲基甲酰胺 110～120℃ 光照 90～100℃ 室温
	一种对虾肠道微生物DNA的提取方法专利 OAI收割专利类型: 发明, 专利号: CN200910263665.0, 申请日期: 2010-06-23, 公开日期: 2010-06-23 刘淮德; 王雷; 刘梅; 王宝杰; 蒋克勇收藏 \| 浏览/下载：31/0 \| 提交时间：2014/08/04 一种对虾肠道微生物DNA的提取方法 2)将洗脱液在200g离心5-10min 沉淀中加0.8-1.2mL?PBS以200g离心取上清菌液 3)将步骤2)所得上清菌液以1200g离心5-10min 4)将步骤3)所得上清菌液中加100-150μLCTAB提取液和10-15μL溶菌酶而后加15-20μL?20％(W/C)SDS和10-15μL蛋白酶K 5)将水浴后菌液在4℃?3200g离心8-15min 6)将水浴后菌液以3200g离心8-15min 7)将步骤6)所得上清菌液中加上清菌液体积0.6-0.8倍的异丙醇 8)将步骤7)所得沉淀中加入600-800μL?70％预冷乙醇其特征在于：1)将0.01-0.05g对虾肠道在液氮下研磨取上清菌液待用将两次离心所得上清菌液合并收集上清菌液放入37℃摇床 60-70℃水浴1-2h 取上清菌液取上清菌液而后于-20℃静置1-2h 14000g离心10-15min 并加入0.8-1.2mL?PBS 合并上清液以300g离心5-10min 振荡30-40min 而后加100-150μL?CTAB液和20-25μL?20％SDS混匀后而后加入与上述上清菌液等体积的酚/氯仿混合液再以4℃?14000g离心10-15min 所得沉淀即为对虾肠道微生物DNA。 15-25μL?PVPP匀浆和200-300μL?0.5％Tween-80 取上清菌液待用涡旋 14000g离心10-15min 所得沉淀待用均匀后吹打洗脱3-5min 60-70℃水浴10-15min 取上清菌液待用
	一种溴酚类PTP1B抑制剂的化学合成方法专利 OAI收割专利类型: 发明, 专利号: CN200810016801.1, 申请日期: 2009-12-09, 公开日期: 2009-12-09 史大永; 李敬; 韩丽君; 郭书举; 袁毅收藏 \| 浏览/下载：33/0 \| 提交时间：2014/08/04 1.一种溴酚类PTP1B抑制剂的化学合成方法 (b)溴素(溴素∶化合物3摩尔比＝2∶1) (c)溴素(溴素∶化合物4摩尔比＝4∶1) (d)三氟乙酸 (e)三溴化硼其特征在于：所述的化合物合成路线为：Scheme 1(a)多聚磷酸乙酸三氯化铝三乙基硅烷二氯甲烷 75～85℃ 室温乙酸室温室温。 50～70min 75～85℃
	Design of the infrared dual-band athermalized optical system based on HDE (EI CONFERENCE) 会议论文 OAI收割 International Symposium on Photoelectronic Detection and Imaging 2009: Advances in Infrared Imaging and Applications, June 17, 2009 - June 19, 2009, Beijing, China 作者: Zhang L.; Sun Q.; Wang H.; Wang H.; Wang H. 收藏 \| 浏览/下载：97/0 \| 提交时间：2013/03/25 A dual-band infrared optical system adopting an uncooled LW infrared detector and a cooled MW infrared detector is designed and manufactured while in the LW IR band the F/# is 1 and the focal length is 114 mm based on the athermal ability and special diffractive properties of harmonic diffractive elements. The design shows in the MW IR band the F/# is 2 and the focal length is 72 mm for the temperature range -40 70 the MTF value is over 0.5 at 10 lp/mm. Finite element method is applied to the opto-mechanic structure of the system for thermal analysis for the temperature range -40C 70C the MTF value is over 0.4 at 20 lp/mm which confirms the imaging ability of the system in a wide temperature range. 2009 SPIE.
	Replacement of methane from quartz sand-bearing hydrate with carbon dioxide-in-water emulsion 期刊论文 OAI收割 energy & fuels, 2008, 卷号: 22, 期号: 3, 页码: 1759-1764 作者: Zhou, Xitang; Fan, Shuanshi; Liang, Deqing; Du, Jianwei 收藏 \| 浏览/下载：79/10 \| 提交时间：2010/09/23 The replacement of CH4 from its hydrate in quartz sand with 90:10, 70:30, and 50:50 (W-CO2:W-H2O) carbon dioxide-in-water (C/W) emulsions and liquid CO2 has been performed in a cell with size of empty set 36 x 200 mm. The above emulsions were formed in a new emulsifier, in which the temperature and pressure were 285.2 K and 30 MPa, respectively, and the emulsions were stable for 7-12 h. The results of replacing showed that 13.1-27.1%, 14.1-25.5%, and 14.6-24.3% of CH4 had been displaced from its hydrate with the above emulsions after 24-96 It of replacement, corresponding to about 1.5 times the CH4 replaced with high-pressure liquid CO2. The results also showed that the replacement rate of CH4 with the above emulsions and liquid CO2 decreased from 0.543, 0.587, 0.608, and 0.348 1/h to 0.083, 0.077, 0.069, and 0.063 1/h with the replacement time increased from 24 to 96 h. It has been indicated by this study that the use of CO2 emulsions is advantageous compared to the use of liquid CO2 in replacing CH4 from its hydrate.
	STUDY OF PHOTOCHEMICAL-REACTION FROM C-70 ADSORBED ON SILVER FILM BY SURFACE-ENHANCED RAMAN-SCATTERING 期刊论文 OAI收割 APPLIED PHYSICS LETTERS, 1995, 卷号: 66, 期号: 19, 页码: 2591 MO, YJ; MATTEI, G; PAGANNONE, M; XIE, SS 收藏 \| 浏览/下载：9/0 \| 提交时间：2013/09/24 VIBRATIONAL RAMAN C60 C-60 SPECTROSCOPY FULLERENE O2 TEMPERATURE SPECTRA GOLD C70